(S)-3-benzyloxybutanoic acid piperidineamide

Base Information

Chemical Name:(S)-3-benzyloxybutanoic acid piperidineamide
CAS No.:124558-79-8
Molecular Formula:C₁₆H₂₃NO₂
Molecular Weight:261.364
Hs Code.:

Synonyms:

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Chemical Property of (S)-3-benzyloxybutanoic acid piperidineamide

Chemical Property:

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Technology Process of (S)-3-benzyloxybutanoic acid piperidineamide

There total 3 articles about (S)-3-benzyloxybutanoic acid piperidineamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-39-0
benzyl bromide

: 124558-79-8
(S)-3-benzyloxybutanoic acid piperidineamide

Guidance literature:: Multi-step reaction with 3 steps

1: 31 percent / silver oxide / diethyl ether

2: 65 percent / hydrazine hydrate / ethanol / 12 h / 0 °C

3: 1.) t-butylnitrite / 1.) 2.9 N hydrochloric/tetrahydrofuran, -30 deg C, 20 min, 2.) ethyl acetate, 0 deg C, 20 h

With tert.-butylnitrite; hydrazine hydrate; silver(l) oxide; In diethyl ether; ethanol;
DOI:10.1016/0022-328X(89)87277-8

Reference yield:

: 112068-33-4
(R)-3-(benzyloxy)butanoic acid ethyl ester

: 124558-79-8
(S)-3-benzyloxybutanoic acid piperidineamide

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / hydrazine hydrate / ethanol / 12 h / 0 °C

2: 1.) t-butylnitrite / 1.) 2.9 N hydrochloric/tetrahydrofuran, -30 deg C, 20 min, 2.) ethyl acetate, 0 deg C, 20 h

With tert.-butylnitrite; hydrazine hydrate; In ethanol;
DOI:10.1016/0022-328X(89)87277-8

Reference yield:

: 110-89-4
piperidine

: (S)-3-Benzyloxy-butyric acid hydrazide

: 124558-79-8
(S)-3-benzyloxybutanoic acid piperidineamide

Guidance literature:: With tert.-butylnitrite; Yield given. Multistep reaction; 1.) 2.9 N hydrochloric/tetrahydrofuran, -30 deg C, 20 min, 2.) ethyl acetate, 0 deg C, 20 h;
DOI:10.1016/0022-328X(89)87277-8