C₁₄H₁₄FIN₄O₄

Base Information

Chemical Name:C₁₄H₁₄FIN₄O₄
CAS No.:1609550-54-0
Molecular Formula:C₁₄H₁₄FIN₄O₄
Molecular Weight:448.192
Hs Code.:

C<sub>14</sub>H<sub>14</sub>FIN<sub>4</sub>O<sub>4</sub>

Synonyms:

Suppliers and Price of C₁₄H₁₄FIN₄O₄

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₁₄H₁₄FIN₄O₄

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₁₄H₁₄FIN₄O₄

There total 4 articles about C₁₄H₁₄FIN₄O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 737747-44-3
C₃H₉NO₃

: 1609550-47-1
C₁₁H₇FIN₃O₂

: 1609550-54-0
C₁₄H₁₄FIN₄O₄

Guidance literature:: With triethylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In tetrahydrofuran; at 20 ℃; for 1h;
DOI:10.1016/j.bmcl.2014.03.086

Reference yield:

: 64224-59-5
ethyl 5-bromopyrimidine-4-carboxylate

: 1609550-54-0
C₁₄H₁₄FIN₄O₄

Guidance literature:: Multi-step reaction with 4 steps

1: palladium diacetate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; caesium carbonate / N,N-dimethyl-formamide / 80 °C

2: N-iodo-succinimide; trifluoroacetic acid / N,N-dimethyl-formamide / 2 h / 80 °C

3: sodium hydroxide / methanol / 20 °C

4: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; triethylamine / tetrahydrofuran / 1 h / 20 °C

With N-iodo-succinimide; palladium diacetate; caesium carbonate; triethylamine; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; trifluoroacetic acid; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; sodium hydroxide; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2014.03.086

Reference yield:

: 1609550-45-9
C₁₃H₁₂FN₃O₂

: 1609550-54-0
C₁₄H₁₄FIN₄O₄

Guidance literature:: Multi-step reaction with 3 steps

1: N-iodo-succinimide; trifluoroacetic acid / N,N-dimethyl-formamide / 2 h / 80 °C

2: sodium hydroxide / methanol / 20 °C

3: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; triethylamine / tetrahydrofuran / 1 h / 20 °C

With N-iodo-succinimide; triethylamine; trifluoroacetic acid; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; sodium hydroxide; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2014.03.086