[Pd₂Cl₃(C₄N₂H₃(C₆H₄))(C₄N₂H₃(C₆H₅))]

Base Information

Chemical Name:[Pd₂Cl₃(C₄N₂H₃(C₆H₄))(C₄N₂H₃(C₆H₅))]
CAS No.:108115-90-8
Molecular Formula:C₂₀H₁₅Cl₃N₄Pd₂
Molecular Weight:630.565
Hs Code.:

[Pd<sub>2</sub>Cl<sub>3</sub>(C<sub>4</sub>N<sub>2</sub>H<sub>3</sub>(C<sub>6</sub>H<sub>4</sub>))(C<sub>4</sub>N<sub>2</sub>H<sub>3</sub>(C<sub>6</sub>H<sub>5</sub>))]

Synonyms:

Suppliers and Price of [Pd₂Cl₃(C₄N₂H₃(C₆H₄))(C₄N₂H₃(C₆H₅))]

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Chemical Property of [Pd₂Cl₃(C₄N₂H₃(C₆H₄))(C₄N₂H₃(C₆H₅))]

Chemical Property:

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Technology Process of [Pd₂Cl₃(C₄N₂H₃(C₆H₄))(C₄N₂H₃(C₆H₅))]

There total 1 articles about [Pd₂Cl₃(C₄N₂H₃(C₆H₄))(C₄N₂H₃(C₆H₅))] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108208-58-8
[PdCl₂(C₄N₂H₃(C₆H₅))2]

: palladium dichloride

: 108115-90-8
[Pd₂Cl₃(C₄N₂H₃(C₆H₄))(C₄N₂H₃(C₆H₅))]

Guidance literature:: In water; acetone; monomeric complex (1mmole) was given an addn. of PdCl2 (1mmole), water (20ml) and acetone (80ml), the mixture was boiled with magnetic stirringand a constant volume for 4h;; the formed yellow ppt. was filtd. out, washed out with acetone and water and dried at 105°C; elem. anal.;;

Reference yield:

: 108115-90-8
[Pd₂Cl₃(C₄N₂H₃(C₆H₄))(C₄N₂H₃(C₆H₅))]

: 107-15-3,85404-18-8
ethylenediamine

: 16483-18-4
bis(ethylenediamine)palladium(II) chloride

: 108115-91-9
[Pd(C₄N₂H₃(C₆H₄))(NH₂CH₂CH₂NH₂)]⁽¹⁺⁾*Cl^(1-)=[Pd(C₄N₂H₃(C₆H₄))(NH₂CH₂CH₂NH₂)]Cl

Guidance literature:: In acetone; byproducts: 4-phenyl pyrimidine; ethylene diamine (9mmole) and acetone (10ml) were given to the corresponding dimeric complex (1mmole), the yellow ppt. instantly transformed itself into a white ppt.;; ppt. was filtd., washed, and heated; on cooling down, an acicular ppt. was formed, that was further filtered, washed and dried at 105°C;by evapn. of aq. filtrate, the di-ethylendiamine complex was obtained; elem. anal.;;

Reference yield:

: 108115-90-8
[Pd₂Cl₃(C₄N₂H₃(C₆H₄))(C₄N₂H₃(C₆H₅))]

: 2Pd⁽²⁺⁾*2Cl^(1-)*2(C₄N₂H₃(C₆H₄))^(1-)=[Pd₂Cl₂(C₄N₂H₃(C₆H₄))2]

Guidance literature:: In water; dimethyl sulfoxide; addn. of watrer to a soln. of dimeric complex in DMSO (the DMSO:H2O ratio was 1:1 by volume);; formation of a yellow ppt. whose composition is a mixture of 75% dichloro and 25% unreacted trichloro complex;;