dicarbonyl(η5-cyclopentadienyl)[N,N-bis(diphenylphosphino)glycine methyl ester-P,P']molybdenum(II) chloride

Base Information

• Chemical Name: dicarbonyl(η5-cyclopentadienyl)[N,N-bis(diphenylphosphino)glycine methyl ester-P,P']molybdenum(II) chloride
• CAS No.: 87686-27-9
• Molecular Formula: C₃₄H₃₀MoNO₄P₂*Cl
• Molecular Weight: 709.957
• Mol file: 87686-27-9.mol

Synonyms:

Chemical Property of dicarbonyl(η5-cyclopentadienyl)[N,N-bis(diphenylphosphino)glycine methyl ester-P,P']molybdenum(II) chloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of dicarbonyl(η5-cyclopentadienyl)[N,N-bis(diphenylphosphino)glycine methyl ester-P,P']molybdenum(II) chloride

There total 1 articles about dicarbonyl(η5-cyclopentadienyl)[N,N-bis(diphenylphosphino)glycine methyl ester-P,P']molybdenum(II) chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

tricarbonylcyclopentadienylmolybdenum(II) chloride (12128-23-3) + ((C6H5)2P)2NCH2C(O)OCH3 (60048-75-1) → dicarbonyl(η5-cyclopentadienyl)[N,N-bis(diphenylphosphino)glycine methyl ester-P,P']molybdenum(II) chloride (87686-27-9)

Guidance literature:

In toluene; byproducts: CO; a mixt. of CpMo(CO)3Cl and (Ph2P)2NCH2COOMe in toluene was stirred under N2 at 70°C for 1 h; the reaction mixt. was cooled, filtered, ppt. was washed with toluene and ether and dried; elem. anal.;

DOI:10.1016/0022-328X(83)80060-6

upstream raw materials:

tricarbonylcyclopentadienylmolybdenum(II) chloride

((C₆H₅)2P)2NCH₂C(O)OCH₃