dichlorobis[η(5)-(pentafluorophenyl)cyclopentadienyl]zirconium(IV)

Base Information

Chemical Name:dichlorobis[η(5)-(pentafluorophenyl)cyclopentadienyl]zirconium(IV)
CAS No.:184481-08-1
Molecular Formula:C₂₂H₈Cl₂F₁₀Zr
Molecular Weight:624.42
Hs Code.:

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Chemical Property of dichlorobis[η(5)-(pentafluorophenyl)cyclopentadienyl]zirconium(IV)

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Technology Process of dichlorobis[η(5)-(pentafluorophenyl)cyclopentadienyl]zirconium(IV)

There total 2 articles about dichlorobis[η(5)-(pentafluorophenyl)cyclopentadienyl]zirconium(IV) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 21959-01-3,125410-70-0,125410-71-1
zirconium tetrachloride bis(tetrahydrofuran) complex

: sodium (pentafluorophenyl)cyclopentadienide

: 184481-08-1
dichlorobis[η(5)-(pentafluorophenyl)cyclopentadienyl]zirconium(IV)

Guidance literature:: In toluene; N2-atmosphere; stirring (100°C, 1 h); filtering, washing (toluene), crystn. (room temp.), filtering, washing (pentane); elem. anal.;
DOI:10.1021/om9608216

Reference yield:

: 602335-46-6
1,1'-bis(pentafluorophenyl)zirconocene dimethide

: 76-83-5
trityl chloride

: 184481-08-1
dichlorobis[η(5)-(pentafluorophenyl)cyclopentadienyl]zirconium(IV)

: 651299-97-7
[(C₆F₅C₅H₄)2Zr(CH₃)Cl]

Guidance literature:: In benzene-d6; byproducts: Ph3CCH3; N2 glovebox; Zr complex was treated with Ph3CCl (1-1.1 equiv.) in benzene-d6 at 60°C for 18 h; NMR monitoring; not isolated;
DOI:10.1021/om0305014

Reference yield: 82.0%

: 184481-08-1
dichlorobis[η(5)-(pentafluorophenyl)cyclopentadienyl]zirconium(IV)

: 917-54-4
methyllithium

: 602335-46-6
1,1'-bis(pentafluorophenyl)zirconocene dimethide

Guidance literature:: In toluene; (N2); stirring a mixt. of zirconium complex with lithium compd. in toluene at 25°C for 18 h in the dark; evapn., recrystn. (hexanes);
DOI:10.1021/om030171n