[2-(η5-dimethylcyclopentadienyl)C6H4NPPh2-κ2N,P]TiCl2

Base Information

Chemical Name:[2-(η5-dimethylcyclopentadienyl)C6H4NPPh2-κ2N,P]TiCl2
CAS No.:922144-01-2
Molecular Formula:C₂₅H₂₂Cl₂NPTi
Molecular Weight:486.216
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Chemical Property of [2-(η5-dimethylcyclopentadienyl)C6H4NPPh2-κ2N,P]TiCl2

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Technology Process of [2-(η5-dimethylcyclopentadienyl)C6H4NPPh2-κ2N,P]TiCl2

There total 1 articles about [2-(η5-dimethylcyclopentadienyl)C6H4NPPh2-κ2N,P]TiCl2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 922144-08-9
[2-(η5-dimethylcyclopentadienyl)C6H4NPPh2-κN]Ti(dimethylamido)2

: 75-78-5,30107-43-8
dimethylsilicon dichloride

: 922144-01-2
[2-(η5-dimethylcyclopentadienyl)C6H4NPPh2-κ2N,P]TiCl2

Guidance literature:: In benzene; using Schlenk techniques; addn. of Me2SiCl2 to flask with soln. of (Ph2PNC6H4C5H2Me2)Ti(NMe2)2 in benzene; stirring for 3 h at room temp.; removal of volatiles under vac.; dissolving in CHCl3; filtration over Celite; removal of solvent; trituration in pentane; elem. anal.;