[2-(η5-dimethylcyclopentadienyl)C6H4NPPh2-κN]Ti(dimethylamido)2

Base Information

Chemical Name:[2-(η5-dimethylcyclopentadienyl)C6H4NPPh2-κN]Ti(dimethylamido)2
CAS No.:922144-08-9
Molecular Formula:C₂₉H₃₄N₃PTi
Molecular Weight:503.463
Hs Code.:

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Chemical Property of [2-(η5-dimethylcyclopentadienyl)C6H4NPPh2-κN]Ti(dimethylamido)2

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Technology Process of [2-(η5-dimethylcyclopentadienyl)C6H4NPPh2-κN]Ti(dimethylamido)2

There total 1 articles about [2-(η5-dimethylcyclopentadienyl)C6H4NPPh2-κN]Ti(dimethylamido)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 922143-95-1
(C₆H₅)2PNHC₆H₄C₅H₃(CH₃)2

: tetrakis(dimethylamido)titanium(IV)

: 922144-08-9
[2-(η5-dimethylcyclopentadienyl)C6H4NPPh2-κN]Ti(dimethylamido)2

Guidance literature:: In benzene; using Schlenk techniques; addn. of Ph2PNHC6H4C5H3Me2, Ti(NMe2)4 and benzene into sealed tube; stirring overnight at 80°C; removal of solvent; recrystn. in pentane at -30°C;

Reference yield: 72.0%

: 922144-08-9
[2-(η5-dimethylcyclopentadienyl)C6H4NPPh2-κN]Ti(dimethylamido)2

: 75-78-5,30107-43-8
dimethylsilicon dichloride

: 922144-01-2
[2-(η5-dimethylcyclopentadienyl)C6H4NPPh2-κ2N,P]TiCl2

Guidance literature:: In benzene; using Schlenk techniques; addn. of Me2SiCl2 to flask with soln. of (Ph2PNC6H4C5H2Me2)Ti(NMe2)2 in benzene; stirring for 3 h at room temp.; removal of volatiles under vac.; dissolving in CHCl3; filtration over Celite; removal of solvent; trituration in pentane; elem. anal.;