Technology Process of 2-benzyloxy-3,5-diethoxy-4-methylbenzaldehyde
There total 1 articles about 2-benzyloxy-3,5-diethoxy-4-methylbenzaldehyde which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 43 percent / acetic acid / 2 h / 135 - 145 °C
2: 98 percent / K2CO3 / dimethylformamide / 48 h / 20 °C
With
potassium carbonate;
In
acetic acid; N,N-dimethyl-formamide;
1: Duff raction;
DOI:10.3987/COM-04-10196
- Guidance literature:
-
Multi-step reaction with 6 steps
1: benzene / 3 h / Heating
2: 9.69 g / NaBH4 / methanol / 1 h / 20 °C
3: 88 percent / pyridine / 20 h / 20 °C
4: aq. HCl / dioxane / 3.5 h / Heating
5: potassium tert-butoxide / 2-methyl-propan-2-ol / 1 h / Heating
6: m-chloroperoxybenzoic acid / CH2Cl2 / 16 h / 20 °C
With
pyridine; hydrogenchloride; sodium tetrahydroborate; potassium tert-butylate; 3-chloro-benzenecarboperoxoic acid;
In
1,4-dioxane; methanol; dichloromethane; tert-butyl alcohol; benzene;
DOI:10.3987/COM-04-10196
- Guidance literature:
-
Multi-step reaction with 5 steps
1: benzene / 3 h / Heating
2: 9.69 g / NaBH4 / methanol / 1 h / 20 °C
3: 88 percent / pyridine / 20 h / 20 °C
4: aq. HCl / dioxane / 3.5 h / Heating
5: potassium tert-butoxide / 2-methyl-propan-2-ol / 1 h / Heating
With
pyridine; hydrogenchloride; sodium tetrahydroborate; potassium tert-butylate;
In
1,4-dioxane; methanol; tert-butyl alcohol; benzene;
DOI:10.3987/COM-04-10196
