Technology Process of C14H16NO3P
There total 10 articles about C14H16NO3P which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: thionyl chloride / 2 h / Heating
2: triethylamine / CH2Cl2 / 1.5 h / Ambient temperature
3: triethylamine / methanol / 0.17 h / 0 °C
4: 53 percent / pyridine / 0.13 h / 0 °C
5: methanol / 0.17 h / 0 °C / migration ratio of phenyl and aryl group
With
thionyl chloride; triethylamine;
In
pyridine; methanol; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: triethylamine / CH2Cl2 / 1.5 h / Ambient temperature
2: triethylamine / methanol / 0.17 h / 0 °C
3: 53 percent / pyridine / 0.13 h / 0 °C
4: methanol / 0.17 h / 0 °C / migration ratio of phenyl and aryl group
With
triethylamine;
In
pyridine; methanol; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: PCl5 / Heating
2: CH2Cl2 / 0 °C / 2 mol equiv. aromatic amine
3: methanol; CH2Cl2
With
phosphorus pentachloride;
In
methanol; dichloromethane;