tricarbonyl[methoxy(o-methoxyphenyl)carbene-κ2C,O](tetrachloro-o-chinolato-κ2O(1,2))tungsten(II)

Base Information

• Chemical Name: tricarbonyl[methoxy(o-methoxyphenyl)carbene-κ2C,O](tetrachloro-o-chinolato-κ2O(1,2))tungsten(II)
• CAS No.: 460989-63-3
• Molecular Formula: C₁₈H₁₀Cl₄O₇W
• Molecular Weight: 663.935

Synonyms:

Chemical Property of tricarbonyl[methoxy(o-methoxyphenyl)carbene-κ2C,O](tetrachloro-o-chinolato-κ2O(1,2))tungsten(II)

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of tricarbonyl[methoxy(o-methoxyphenyl)carbene-κ2C,O](tetrachloro-o-chinolato-κ2O(1,2))tungsten(II)

There total 1 articles about tricarbonyl[methoxy(o-methoxyphenyl)carbene-κ2C,O](tetrachloro-o-chinolato-κ2O(1,2))tungsten(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

o-tetrachloroquinone (2435-53-2) + cis-tetracarbonyl{methoxy-2-phenyl(methoxy)carbene-C,O}tungsten → Pentacarbonyl{methoxy(methoxy-2-phenyl)carben}wolfram + tricarbonyl[methoxy(o-methoxyphenyl)carbene-κ2C,O](tetrachloro-o-chinolato-κ2O(1,2))tungsten(II) (460989-63-3)

Guidance literature:

In dichloromethane; byproducts: CO; (N2); addn. of a soln. of quinone deriv. in CH2Cl2 to a soln. of tungsten complex in CH2Cl2 at -10°C; evapn., chromy. (SiO2, pentane/CH2Cl2, 10:1 to 1:20), evapn.; elem. anal.;

DOI:10.1016/S0022-328X(02)01255-X

upstream raw materials:

o-tetrachloroquinone

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