6,8-diiodo-2-methyl-4H-3,1-benzoxazin-4-one

Base Information

Chemical Name:6,8-diiodo-2-methyl-4H-3,1-benzoxazin-4-one
CAS No.:17987-78-9
Molecular Formula:C₉H₅I₂NO₂
Molecular Weight:412.953
Hs Code.:
DSSTox Substance ID:DTXSID901263745
Mol file:17987-78-9.mol

Synonyms:6,8-diiodo-2-methyl-4H-3,1-benzoxazin-4-one;17987-78-9;6,8-diiodo-2-methyl-3,1-benzoxazin-4-one;SCHEMBL12758389;DTXSID901263745;AKOS003264940;AN-979/15448098;6,8-diiodo-2-methyl-4h-benzo[d][1,3]oxazin-4-one

Suppliers and Price of 6,8-diiodo-2-methyl-4H-3,1-benzoxazin-4-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 6,8-diiodo-2-methyl-4H-3,1-benzoxazin-4-one

Chemical Property:

XLogP3:2.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:0
Exact Mass:412.84097
Heavy Atom Count:14
Complexity:293

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=NC2=C(C=C(C=C2I)I)C(=O)O1

Technology Process of 6,8-diiodo-2-methyl-4H-3,1-benzoxazin-4-one

There total 2 articles about 6,8-diiodo-2-methyl-4H-3,1-benzoxazin-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 108-24-7
acetic anhydride

: 609-86-9
2-amino-3,5-diiodobenzoic acid

: 17987-78-9
6,8-diiodo-2-methyl-4H-benzo[d][1,3]oxazin-4-one

Guidance literature:: for 1h; Reflux;
DOI:10.1007/s00044-013-0569-5

Reference yield:

: 118-92-3,159201-01-1,50816-84-7,80206-34-4,104809-47-4
anthranilic acid

: 17987-78-9
6,8-diiodo-2-methyl-4H-benzo[d][1,3]oxazin-4-one

Guidance literature:: Multi-step reaction with 2 steps

1: aqueous hydrochloric acid; iodine monochloride

2: H₂SO₄

With hydrogenchloride; sulfuric acid; Iodine monochloride;
DOI:10.1021/ja01137a035