1-(CH(o-CB₁₀H₁₀CC₆H₅)OH)-2-(C₆H₅)-1.2-C₂B₁₀H₁₀

Base Information

Chemical Name:1-(CH(o-CB₁₀H₁₀CC₆H₅)OH)-2-(C₆H₅)-1.2-C₂B₁₀H₁₀
CAS No.:16450-20-7
Molecular Formula:C₁₇H₃₂B₂₀O
Molecular Weight:468.66
Hs Code.:

1-(CH(o-CB<sub>10</sub>H<sub>10</sub>CC<sub>6</sub>H<sub>5</sub>)OH)-2-(C<sub>6</sub>H<sub>5</sub>)-1.2-C<sub>2</sub>B<sub>10</sub>H<sub>10</sub>

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Chemical Property of 1-(CH(o-CB₁₀H₁₀CC₆H₅)OH)-2-(C₆H₅)-1.2-C₂B₁₀H₁₀

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Technology Process of 1-(CH(o-CB₁₀H₁₀CC₆H₅)OH)-2-(C₆H₅)-1.2-C₂B₁₀H₁₀

There total 6 articles about 1-(CH(o-CB₁₀H₁₀CC₆H₅)OH)-2-(C₆H₅)-1.2-C₂B₁₀H₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 109-72-8
n-butyllithium

: 16390-61-7
1-phenyl-1,2-closo-C₂B₁₀H₁₁

: 109-94-4
formic acid ethyl ester

: 16450-20-7
1-(CH(o-CB₁₀H₁₀CC₆H₅)OH)-2-(C₆H₅)-1.2-C₂B₁₀H₁₀

Guidance literature:: With hydrogenchloride; In diethyl ether; benzene; nitrogen atmosphere; ether soln. of formate addn. at 50 to 60°C to benzene soln. of Li-salt of carborane (obtained from carborane and BuLi), stirring (1 h), treating with aq. HCl, extracting with ether; extract drying over MgSO4 and evapn., residue recrystn. (hexane);

Reference yield: 80.0%

: 16390-61-7
1-phenyl-1,2-closo-C₂B₁₀H₁₁

: 925-90-6
ethylmagnesium bromide

: 109-94-4
formic acid ethyl ester

: 16450-20-7
1-(CH(o-CB₁₀H₁₀CC₆H₅)OH)-2-(C₆H₅)-1.2-C₂B₁₀H₁₀

Guidance literature:: With ammonium chloride; In tetrahydrofuran; nitrogen atmosphere; THF soln. of formate addn. at 50 to 60°C to soln. of MgBr-salt of carborane (obtained from carborane and EtMgBr), stirring (1 h), treating with aq. NH4Cl, extracting with ether; extract drying over MgSO4 and evapn., residue recrystn. (hexane);

Reference yield: 60.0%

: 18972-17-3
1-(MgBr)-2-(C₆H₅)-1.2-C₂B₁₀H₁₀

: 109-94-4
formic acid ethyl ester

: 12082-52-9
1-CHO-2-C₆H₅-1.2-C₂B₁₀H₁₀

: 16450-20-7
1-(CH(o-CB₁₀H₁₀CC₆H₅)OH)-2-(C₆H₅)-1.2-C₂B₁₀H₁₀

Guidance literature:: With ammonium chloride; In tetrahydrofuran; nitrogen atmosphere; MgBr-salt of carborane addn. to soln. of formate at-30 to -70°C, stirring (2 h, -30°C), treating with aq. NH 4Cl, extracting with ether; extract drying over MgSO4 and evapn., residue recrystn. (hexane);