2-methyl-2-{[(4-methylphenyl)sulfonyl]amino}propane-1,3-diyl bis(4-methylbenzenesulfonate)

Base Information

• Chemical Name: 2-methyl-2-{[(4-methylphenyl)sulfonyl]amino}propane-1,3-diyl bis(4-methylbenzenesulfonate)
• CAS No.: 10405-52-4
• Molecular Formula: C25H29 N O8 S3
• Molecular Weight: 567.6947
• Mol file: 10405-52-4.mol

Synonyms:p-Toluenesulfonamide, N-[1,1-bis(hydroxymethyl)ethyl]-,di-p-toluenesulfonate (7CI,8CI); NSC 240537

Chemical Property of 2-methyl-2-{[(4-methylphenyl)sulfonyl]amino}propane-1,3-diyl bis(4-methylbenzenesulfonate)

Chemical Property:

• Vapor Pressure: 8.08E-22mmHg at 25°C
• Boiling Point: 740.9°Cat760mmHg
• Flash Point: 401.9°C
• Density: 1.34g/cm³

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-methyl-2-{[(4-methylphenyl)sulfonyl]amino}propane-1,3-diyl bis(4-methylbenzenesulfonate)

There total 1 articles about 2-methyl-2-{[(4-methylphenyl)sulfonyl]amino}propane-1,3-diyl bis(4-methylbenzenesulfonate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

p-toluenesulfonyl chloride (98-59-9) + 2-Amino-2-methylpropane-1,3-diol (115-69-5) → N-(1,1-bis(hydroxymethyl)ethyl)-p-toluenesulfonamide, di-p-toluenesulfonate (10405-52-4)

Guidance literature:

With pyridine; at 0 ℃; Cooling;

DOI:10.1021/jo100640w

Reference yield: 91.0%

N-(1,1-bis(hydroxymethyl)ethyl)-p-toluenesulfonamide, di-p-toluenesulfonate (10405-52-4) → C18H21NO5S2

Guidance literature:

With potassium carbonate; In acetonitrile; at 20 ℃;

DOI:10.1021/jo100640w

Reference yield:

N-(1,1-bis(hydroxymethyl)ethyl)-p-toluenesulfonamide, di-p-toluenesulfonate (10405-52-4) + potassium thioacetate (10387-40-3) → thio-acetic acid, S,S'-diester with N-(1,1-bis(mercaptomethyl)ethyl)-p-toluenesulfonamide (10405-54-6)

Guidance literature:

In acetone;

DOI:10.1021/jm00322a026

upstream raw materials:

p-toluenesulfonyl chloride

2-Amino-2-methylpropane-1,3-diol

Downstream raw materials:

thio-acetic acid, S,S'-diester with N-(1,1-bis(mercaptomethyl)ethyl)-p-toluenesulfonamide

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