triphenylphosphonium bis(diphenylstibino)methylide

Base Information

Chemical Name:triphenylphosphonium bis(diphenylstibino)methylide
CAS No.:87482-32-4
Molecular Formula:C₄₃H₃₅PSb₂
Molecular Weight:826.225
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of triphenylphosphonium bis(diphenylstibino)methylide

Chemical Property:

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Technology Process of triphenylphosphonium bis(diphenylstibino)methylide

There total 3 articles about triphenylphosphonium bis(diphenylstibino)methylide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 2629-47-2
diphenylantimony(III) chloride

: 19493-09-5
Methylenetriphenylphosphorane

: 87482-32-4
triphenylphosphonium bis(diphenylstibino)methylide

Guidance literature:: In toluene; byproducts: Ph3PCH3Cl; (N2); (C6H5)2SbCl soln. added dropwise to stirred soln. of (C6H5)3PCH2 in molar ratio 2/3 at 70°C, stirred for 3 h; ppt. washed with toluene, solvent removed in vac., residue washed with toluene, then with pentane, dried (vac.); elem. anal.;
DOI:10.1021/om00079a009

Reference yield:

: 59-88-1
phenylhydrazine hydrochloride

: 87482-32-4
triphenylphosphonium bis(diphenylstibino)methylide

Guidance literature:: Multi-step reaction with 3 steps

1: CuCl₂; O₂ / not given

2: disulfite or SnCl₂ / further solvent(s)

3: toluene

With CuCl₂; O₂; disulfite or SnCl₂; In toluene;
DOI:10.1021/om00079a009

Reference yield:

: diphenylstibine trichloride hydrate

: 87482-32-4
triphenylphosphonium bis(diphenylstibino)methylide

Guidance literature:: Multi-step reaction with 2 steps

1: disulfite or SnCl₂ / further solvent(s)

2: toluene

With disulfite or SnCl₂; In toluene;
DOI:10.1021/om00079a009