Li(OC₄H₈)4⁽¹⁺⁾*Sn₃(NC₄H₉)(C₁₀H₇N)3Li(OC₄H₈)^(1-)*C₄H₈O*C₇H₈ = [Li(OC₄H₈)4][Sn₃(NC₄H₉)(C₁₀H₇N)3Li(OC₄H₈)]*C₄H₈O*C₇H₈

Base Information

• Chemical Name: Li(OC₄H₈)4⁽¹⁺⁾*Sn₃(NC₄H₉)(C₁₀H₇N)3Li(OC₄H₈)^(1-)*C₄H₈O*C₇H₈ = [Li(OC₄H₈)4][Sn₃(NC₄H₉)(C₁₀H₇N)3Li(OC₄H₈)]*C₄H₈O*C₇H₈
• CAS No.: 180839-26-3
• Molecular Formula: C₄H₈O*C₇H₈*C₁₆H₃₂LiO₄*C₃₈H₃₈LiN₄OSn₃
• Molecular Weight: 1389.43
• Mol file: 180839-26-3.mol

Synonyms:

Chemical Property of Li(OC₄H₈)4⁽¹⁺⁾*Sn₃(NC₄H₉)(C₁₀H₇N)3Li(OC₄H₈)^(1-)*C₄H₈O*C₇H₈ = [Li(OC₄H₈)4][Sn₃(NC₄H₉)(C₁₀H₇N)3Li(OC₄H₈)]*C₄H₈O*C₇H₈

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Li(OC₄H₈)4⁽¹⁺⁾*Sn₃(NC₄H₉)(C₁₀H₇N)3Li(OC₄H₈)^(1-)*C₄H₈O*C₇H₈ = [Li(OC₄H₈)4][Sn₃(NC₄H₉)(C₁₀H₇N)3Li(OC₄H₈)]*C₄H₈O*C₇H₈

There total 1 articles about Li(OC₄H₈)4⁽¹⁺⁾*Sn₃(NC₄H₉)(C₁₀H₇N)3Li(OC₄H₈)^(1-)*C₄H₈O*C₇H₈ = [Li(OC₄H₈)4][Sn₃(NC₄H₉)(C₁₀H₇N)3Li(OC₄H₈)]*C₄H₈O*C₇H₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

tetrahydrofuran (109-99-9,24979-97-3,77392-70-2) + N-lithio 1-aminonaphthalene (30897-53-1,137059-03-1) + tin(II) dimethylamide (55853-40-2) + tert-butylamine (75-64-9) → Li(OC4H8)4(1+)*Sn3(NC4H9)(C10H7N)3Li(OC4H8)(1-)*C4H8O*C7H8 = [Li(OC4H8)4][Sn3(NC4H9)(C10H7N)3Li(OC4H8)]*C4H8O*C7H8 (180839-26-3)

Guidance literature:

In tetrahydrofuran; toluene; reaction of the Sn compd. with t-BuNH2 in toluene, heating to reflux (toin situ prepare a Sn/N cubane derivative), addn. to C10H7NHLi (prepd. f rom C10H7NH2 and n-BuLi) in toluene/THF, reflux (20 min); filtration (Celite), addn. of hexane, heating for soln., crystn. on storage (5°C, 48 h);

DOI:10.1039/cc9960001501

upstream raw materials:

tetrahydrofuran

N-lithio 1-aminonaphthalene

tin(II) dimethylamide

tert-butylamine