C₂₉H₂₀O₂S

Base Information

Chemical Name:C₂₉H₂₀O₂S
CAS No.:226089-82-3
Molecular Formula:C₂₉H₂₀O₂S
Molecular Weight:432.543
Hs Code.:

C<sub>29</sub>H<sub>20</sub>O<sub>2</sub>S

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₉H₂₀O₂S

Chemical Property:

Purity/Quality:

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Technology Process of C₂₉H₂₀O₂S

There total 12 articles about C₂₉H₂₀O₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 226089-80-1
2-(2-benzenesulfonylmethyl-phenyl)-[1,3]dioxolane

: 226089-82-3
C₂₉H₂₀O₂S

Guidance literature:: Multi-step reaction with 11 steps

1.1: BuLi / tetrahydrofuran; hexane / 1 h / -78 °C

1.2: tetrahydrofuran; hexane / 1 h / -78 °C

2.1: tetrahydrofuran; hexane / 2 h

3.1: t-BuOK / tetrahydrofuran; hexane / 3.67 h / 0 - 20 °C

4.1: 98 percent / p-TsOH; H₂O / acetone / 16 h / 40 °C

5.1: BuLi / tetrahydrofuran; hexane / 1 h / -78 °C

5.2: tetrahydrofuran; hexane / 20 °C

6.1: tetrahydrofuran; hexane / 20 °C

7.1: t-BuOK / tetrahydrofuran; hexane / 20 °C

8.1: p-TsOH; H₂O / acetone

9.1: NaBH₄

10.1: PBr₃

11.1: dimethylformamide

With sodium tetrahydroborate; n-butyllithium; potassium tert-butylate; water; phosphorus tribromide; toluene-4-sulfonic acid; In tetrahydrofuran; hexane; N,N-dimethyl-formamide; acetone; 1.1: Metallation / 1.2: Addition / 2.1: Substitution / 3.1: Elimination / 4.1: Hydrolysis / 5.1: Metallation / 5.2: Addition / 6.1: Substitution / 7.1: Elimination / 8.1: Hydrolysis / 9.1: Reduction / 10.1: Substitution / 11.1: Substitution;

Reference yield:

: 468751-38-4
ortho-(phenylsulfonylmethyl)benzaldehyde

: 226089-82-3
C₂₉H₂₀O₂S

Guidance literature:: Multi-step reaction with 12 steps

1.1: TMSOTf

2.1: BuLi / tetrahydrofuran; hexane / 1 h / -78 °C

2.2: tetrahydrofuran; hexane / 1 h / -78 °C

3.1: tetrahydrofuran; hexane / 2 h

4.1: t-BuOK / tetrahydrofuran; hexane / 3.67 h / 0 - 20 °C

5.1: 98 percent / p-TsOH; H₂O / acetone / 16 h / 40 °C

6.1: BuLi / tetrahydrofuran; hexane / 1 h / -78 °C

6.2: tetrahydrofuran; hexane / 20 °C

7.1: tetrahydrofuran; hexane / 20 °C

8.1: t-BuOK / tetrahydrofuran; hexane / 20 °C

9.1: p-TsOH; H₂O / acetone

10.1: NaBH₄

11.1: PBr₃

12.1: dimethylformamide

With sodium tetrahydroborate; n-butyllithium; trimethylsilyl trifluoromethanesulfonate; potassium tert-butylate; water; phosphorus tribromide; toluene-4-sulfonic acid; In tetrahydrofuran; hexane; N,N-dimethyl-formamide; acetone; 1.1: Etherification / 2.1: Metallation / 2.2: Addition / 3.1: Substitution / 4.1: Elimination / 5.1: Hydrolysis / 6.1: Metallation / 6.2: Addition / 7.1: Substitution / 8.1: Elimination / 9.1: Hydrolysis / 10.1: Reduction / 11.1: Substitution / 12.1: Substitution;

Reference yield:

: 2-benzenesulfonyl-2-(2-[1,3]dioxolan-2-yl-phenyl)-1-phenyl-ethanol

: 226089-82-3
C₂₉H₂₀O₂S

Guidance literature:: Multi-step reaction with 10 steps

1.1: tetrahydrofuran; hexane / 2 h

2.1: t-BuOK / tetrahydrofuran; hexane / 3.67 h / 0 - 20 °C

3.1: 98 percent / p-TsOH; H₂O / acetone / 16 h / 40 °C

4.1: BuLi / tetrahydrofuran; hexane / 1 h / -78 °C

4.2: tetrahydrofuran; hexane / 20 °C

5.1: tetrahydrofuran; hexane / 20 °C

6.1: t-BuOK / tetrahydrofuran; hexane / 20 °C

7.1: p-TsOH; H₂O / acetone

8.1: NaBH₄

9.1: PBr₃

10.1: dimethylformamide

With sodium tetrahydroborate; n-butyllithium; potassium tert-butylate; water; phosphorus tribromide; toluene-4-sulfonic acid; In tetrahydrofuran; hexane; N,N-dimethyl-formamide; acetone; 1.1: Substitution / 2.1: Elimination / 3.1: Hydrolysis / 4.1: Metallation / 4.2: Addition / 5.1: Substitution / 6.1: Elimination / 7.1: Hydrolysis / 8.1: Reduction / 9.1: Substitution / 10.1: Substitution;