2-cyano-3-(2'-(5',10',15',20'-tetraphenylporphyrinato zinc(II)yl))acrylic acid

Base Information

Chemical Name:2-cyano-3-(2'-(5',10',15',20'-tetraphenylporphyrinato zinc(II)yl))acrylic acid
CAS No.:866206-33-9
Molecular Formula:C₄₈H₂₉N₅O₂Zn
Molecular Weight:773.181
Hs Code.:

Synonyms:

Suppliers and Price of 2-cyano-3-(2'-(5',10',15',20'-tetraphenylporphyrinato zinc(II)yl))acrylic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-cyano-3-(2'-(5',10',15',20'-tetraphenylporphyrinato zinc(II)yl))acrylic acid

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-cyano-3-(2'-(5',10',15',20'-tetraphenylporphyrinato zinc(II)yl))acrylic acid

There total 3 articles about 2-cyano-3-(2'-(5',10',15',20'-tetraphenylporphyrinato zinc(II)yl))acrylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 866206-34-0
2-cyano-3-(2'-(5',10',15',20'-tetraphenylporphyrinato zinc(II)yl))acrylic acid piperidine salt

: 86119-84-8,7664-38-2
phosphoric acid

: 866206-33-9,911384-94-6
2-cyano-3-(2'-(5',10',15',20'-tetraphenylporphyrinato zinc(II)yl))acrylic acid

Guidance literature:: In dimethylsulfoxide-d6; chloroform; water; under N2 or Ar; shielded from ambient light; Zn porphyrin complex dissolved in DMSO-d6; H2O and CHCl3 added; transfered to separating funnel; 2M H3PO4 (2.0 ml) added; vigorously shaken (pH 2.0); org. layer washed with H2O (150 ml) containing 2 M H3PO4 (1.0 ml); sepn.; CHCl3 removed with azeotrope distn. with CH3CN in vac.; pptn. with H2O;
DOI:10.1021/jp052877w

Reference yield:

: 110350-65-7
2-formyl-5,10,15,20-tetraphenylporphyrinato zinc(II)

: 866206-33-9,911384-94-6
2-cyano-3-(2'-(5',10',15',20'-tetraphenylporphyrinato zinc(II)yl))acrylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: acetonitrile

2: water; chloroform; dimethylsulfoxide-d6

In dimethylsulfoxide-d6; chloroform; water; acetonitrile;
DOI:10.1021/jp052877w

Reference yield:

: 2-formyl-5,10,15,20-tetraphenylporphyrine

: 866206-33-9,911384-94-6
2-cyano-3-(2'-(5',10',15',20'-tetraphenylporphyrinato zinc(II)yl))acrylic acid

Guidance literature:: Multi-step reaction with 3 steps

1: chloroform; methanol

2: acetonitrile

3: water; chloroform; dimethylsulfoxide-d6

In methanol; dimethylsulfoxide-d6; chloroform; water; acetonitrile;
DOI:10.1021/jp052877w