P-(2-(chlorodimethylstannyl)phenyl)-N,N-diisopropyl-P-phenylphosphinothioic amide

Base Information

• Chemical Name: P-(2-(chlorodimethylstannyl)phenyl)-N,N-diisopropyl-P-phenylphosphinothioic amide
• CAS No.: 1388802-94-5
• Molecular Formula: C₂₀H₂₉ClNPSSn
• Molecular Weight: 500.66

Synonyms:

Chemical Property of P-(2-(chlorodimethylstannyl)phenyl)-N,N-diisopropyl-P-phenylphosphinothioic amide

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of P-(2-(chlorodimethylstannyl)phenyl)-N,N-diisopropyl-P-phenylphosphinothioic amide

There total 1 articles about P-(2-(chlorodimethylstannyl)phenyl)-N,N-diisopropyl-P-phenylphosphinothioic amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

N,N-diisopropyl-P,P-diphenylphosphinothioic amide + dimethyltin dichloride (753-73-1) → P-(2-(chlorodimethylstannyl)phenyl)-N,N-diisopropyl-P-phenylphosphinothioic amide (1388802-94-5)

Guidance literature:

With CH₃(CH₂)3Li; (CH₃)2NCH₂CH₂N(CH₃)2; In diethyl ether; hexane; (N2); addn. of 1.5 equiv. of butyllithium in hexane to phosphinothioic acid deriv. and 5 equiv. of diamine deriv. in dry ether at 0°C, keeping for 2 h, addn. of tin compd., stirring at 0°C for 2 h; addn. of methanol, addn. into water, extn. (CH2Cl2), drying over Na2SO4,evapn. in vac., reppn. from diethyl ether, NMR and HRMS;

DOI:10.1039/c2ob25395j

upstream raw materials:

dimethyltin dichloride

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