[dimethylsilanediyl-(9-η5-fluorenyl)(2-phenyl-1-η5-indenyl)]zirconium dichloride

Base Information

Chemical Name:[dimethylsilanediyl-(9-η5-fluorenyl)(2-phenyl-1-η5-indenyl)]zirconium dichloride
CAS No.:301323-16-0
Molecular Formula:C₃₀H₂₄Cl₂SiZr
Molecular Weight:574.736
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [dimethylsilanediyl-(9-η5-fluorenyl)(2-phenyl-1-η5-indenyl)]zirconium dichloride

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Technology Process of [dimethylsilanediyl-(9-η5-fluorenyl)(2-phenyl-1-η5-indenyl)]zirconium dichloride

There total 1 articles about [dimethylsilanediyl-(9-η5-fluorenyl)(2-phenyl-1-η5-indenyl)]zirconium dichloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 28.0%

: 301323-19-3
1-(9-fluorenyl)-1-(2-phenylindenyl)dimethylsilane

: 10026-11-6
zirconium(IV) chloride

: 301323-16-0
[dimethylsilanediyl-(9-η5-fluorenyl)(2-phenyl-1-η5-indenyl)]zirconium dichloride

Guidance literature:: With n-butyllithium; In diethyl ether; toluene; under Ar to 1-(9-fluorenyl)-1-(2-phenylindenyl)ethane in Et2O n-BuLi was added at -78°c, react. was warmed to room temp., stirred for 2 h, solvent was removed, residue was diluted in toluene and ZrCl4 was added at -78°C; soln. was allowed to warm to room temp. and stirred overnight, mixt. was filtered, solid was extd. with toluene, solvent was removed, residue was washed with Et2O and pentane; elem. anal.;
DOI:10.1021/om000224q