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Technology Process of Me2C(3-(2-phenyl-2-adamantyl)-C5H4)(fluorenylidene)ZrCl2

Me2C(3-(2-phenyl-2-adamantyl)-C5H4)(fluorenylidene)ZrCl2

Base Information
  • Chemical Name:Me2C(3-(2-phenyl-2-adamantyl)-C5H4)(fluorenylidene)ZrCl2
  • CAS No.:473174-30-0
  • Molecular Formula:C37H36Cl2Zr
  • Molecular Weight:642.823
  • Hs Code.:
Me<sub>2</sub>C(3-(2-phenyl-2-adamantyl)-C<sub>5</sub>H<sub>4</sub>)(fluorenylidene)ZrCl<sub>2</sub>

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Chemical Property of Me2C(3-(2-phenyl-2-adamantyl)-C5H4)(fluorenylidene)ZrCl2
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Technology Process of Me2C(3-(2-phenyl-2-adamantyl)-C5H4)(fluorenylidene)ZrCl2

There total 1 articles about Me2C(3-(2-phenyl-2-adamantyl)-C5H4)(fluorenylidene)ZrCl2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.8%

Me<sub>2</sub>C(3-(2-phenyl-2-adamantyl)-C<sub>5</sub>H<sub>3</sub>)(fluorenylidene)Li<sub>2</sub>

Me2C(3-(2-phenyl-2-adamantyl)-C5H3)(fluorenylidene)Li2

zirconium(IV) chloride
10026-11-6

zirconium(IV) chloride

Me<sub>2</sub>C(3-(2-phenyl-2-adamantyl)-C<sub>5</sub>H<sub>4</sub>)(fluorenylidene)ZrCl<sub>2</sub>
473174-30-0

Me2C(3-(2-phenyl-2-adamantyl)-C5H4)(fluorenylidene)ZrCl2

Guidance literature:
In petroleum ether; under inert atm. petroleum ether was condensed at -78°C onto mixt. ZrCl4 and Li salt ligand, cold bath was removed, 22 h; solvent was removed, residue was extracted with CH2Cl2 overnight, product was dried in vacuo; elem. anal.;
DOI:10.1021/om050841k
upstream raw materials:

zirconium(IV) chloride

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