Technology Process of C36H60N6O7*ClH
There total 8 articles about C36H60N6O7*ClH which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: tert-butylisonitrile / chloroform / 23 °C / Inert atmosphere
2: hydrogenchloride / 1,4-dioxane / 0.17 h
3: Cyclohexyl isocyanide / chloroform / 23 °C / Inert atmosphere
4: hydrogenchloride / 1,4-dioxane / 0.17 h
5: Cyclohexyl isocyanide / chloroform / 0.75 h / 80 °C / Inert atmosphere; Microwave irradiation
6: hydrogenchloride / 1,4-dioxane / 0.17 h
With
hydrogenchloride; Cyclohexyl isocyanide; tert-butylisonitrile;
In
1,4-dioxane; chloroform;
DOI:10.1021/ja2103372
- Guidance literature:
-
Multi-step reaction with 8 steps
1: tert-butylisonitrile / chloroform / 23 °C / Inert atmosphere
2: hydrogenchloride / 1,4-dioxane / 0.17 h
3: tert-butylisonitrile / chloroform / 23 °C / Inert atmosphere
4: hydrogenchloride / 1,4-dioxane / 0.17 h
5: Cyclohexyl isocyanide / chloroform / 23 °C / Inert atmosphere
6: hydrogenchloride / 1,4-dioxane / 0.17 h
7: Cyclohexyl isocyanide / chloroform / 0.75 h / 80 °C / Inert atmosphere; Microwave irradiation
8: hydrogenchloride / 1,4-dioxane / 0.17 h
With
hydrogenchloride; Cyclohexyl isocyanide; tert-butylisonitrile;
In
1,4-dioxane; chloroform;
DOI:10.1021/ja2103372
- Guidance literature:
-
Multi-step reaction with 5 steps
1: hydrogenchloride / 1,4-dioxane / 0.17 h
2: Cyclohexyl isocyanide / chloroform / 23 °C / Inert atmosphere
3: hydrogenchloride / 1,4-dioxane / 0.17 h
4: Cyclohexyl isocyanide / chloroform / 0.75 h / 80 °C / Inert atmosphere; Microwave irradiation
5: hydrogenchloride / 1,4-dioxane / 0.17 h
With
hydrogenchloride; Cyclohexyl isocyanide;
In
1,4-dioxane; chloroform;
DOI:10.1021/ja2103372