[Ir(tht)(PPh₃)2Cl₃]

Base Information

Chemical Name:[Ir(tht)(PPh₃)2Cl₃]
CAS No.:1375970-02-7
Molecular Formula:C₄₀H₃₈Cl₃IrP₂S
Molecular Weight:911.334
Hs Code.:

[Ir(tht)(PPh<sub>3</sub>)2Cl<sub>3</sub>]

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Chemical Property of [Ir(tht)(PPh₃)2Cl₃]

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Technology Process of [Ir(tht)(PPh₃)2Cl₃]

There total 2 articles about [Ir(tht)(PPh₃)2Cl₃] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 35925-64-5,445022-31-1
[Ir(tetrahydrothiophene)₃Cl₃]

: 603-35-0
triphenylphosphine

: 1375970-02-7
[Ir(tht)(PPh₃)2Cl₃]

Guidance literature:: In decalin; (Ar) mixt. Ir complex and PPh3 (1:2) in decalin was heated to reflux for6 h; react. mixt. was cooled to room temp., solvent was removed in vacuo, residue was triturated with hexane, ppt. was filtered and washed with CH2Cl2; elem. anal.;
DOI:10.1021/om300325y

Reference yield: 24.0%

: 1375970-01-6
Ir(tht)2(PPh₃)Cl₃]

: 603-35-0
triphenylphosphine

: 1375970-02-7
[Ir(tht)(PPh₃)2Cl₃]

Guidance literature:: In decalin; (Ar) mixt. Ir complex and PPh3 in decalin was heated to reflux for 0.5 h; elem. anal.;
DOI:10.1021/om300325y

Reference yield: 35.0%

: 1375970-02-7
[Ir(tht)(PPh₃)2Cl₃]

: 3974-71-8
3-trifluoromethyl-5-(2-pyridyl)pyrazole

: 7650-91-1
benzyldiphenylphosphane

: [Ir(benzyldiphenylphosphine^(1-))(5-pyridyl-3-trifluoromethyl-1H-pyrazole^(1-))2]

Guidance literature:: With Na₂CO₃; In decalin; (Ar) mixt. Ir complex and bdpH in decalin was heated at 180°C for3 h, react. mixt. was cooled to room temp., fppzH and Na2CO3 were added , heated to reflux for 16 h; chromy. on silica (EtOAc-hexane 1:1) and crystn. from CH2Cl2-hexane;
DOI:10.1021/om300325y