O-methylperipentadenine

Base Information

Chemical Name:O-methylperipentadenine
CAS No.:87201-38-5
Molecular Formula:C₂₃H₃₆N₂O₃
Molecular Weight:388.55
Hs Code.:

Synonyms:

Suppliers and Price of O-methylperipentadenine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of O-methylperipentadenine

Chemical Property:

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Technology Process of O-methylperipentadenine

There total 9 articles about O-methylperipentadenine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 126524-13-8
(E)-1-(3-hexanoylaminopropyl)-2-(2-methoxy-6-methylbenzoylmethylene)pyrrolidine

: 87201-38-5,87248-04-2
O-methylperipentadenine

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃;
DOI:10.1016/S0040-4039(01)80533-5

Reference yield:

: 6161-64-4
1-(2-methoxy-6-methylphenyl)ethanone

: 87201-38-5,87248-04-2
O-methylperipentadenine

Guidance literature:: Multi-step reaction with 5 steps

1: 64 percent / 2-pyrrolidone, pyrrolidone hydrotribromide / tetrahydrofuran

2: 2.) triphenylphosphine, triethylamine / 1.) a) 6 h, b) acetone, -23 deg C, 46 h, 2.) acetone, acetonitrile, 40 min

3: nickel-aluminium alloy, aq. NaOH / ethanol / 0.67 h

4: 43 percent / pyridine / 1 h / 0 °C

5: 71 percent / LiAlH₄ / tetrahydrofuran / 1.) 230 min, 2.) -23 deg C, 19 h

With pyridine; 2-pyrrolidinon; sodium hydroxide; lithium aluminium tetrahydride; pyrrolidone hydrotribromide; nickel-aluminium alloy; triethylamine; triphenylphosphine; In tetrahydrofuran; ethanol;
DOI:10.1016/0040-4020(95)01051-3

Reference yield:

: 126524-09-2
2-bromo-1-(2-methoxy-6-methylphenyl)ethanone

: 87201-38-5,87248-04-2
O-methylperipentadenine

Guidance literature:: Multi-step reaction with 4 steps

1: 2.) triphenylphosphine, triethylamine / 1.) a) 6 h, b) acetone, -23 deg C, 46 h, 2.) acetone, acetonitrile, 40 min

2: nickel-aluminium alloy, aq. NaOH / ethanol / 0.67 h

3: 43 percent / pyridine / 1 h / 0 °C

4: 71 percent / LiAlH₄ / tetrahydrofuran / 1.) 230 min, 2.) -23 deg C, 19 h

With pyridine; sodium hydroxide; lithium aluminium tetrahydride; nickel-aluminium alloy; triethylamine; triphenylphosphine; In tetrahydrofuran; ethanol;
DOI:10.1016/0040-4020(95)01051-3