tricarbonyl(η-cyclopentadienyl)(2,3,4,5-tetraphenylstibolyl)molybdenum

Base Information

Chemical Name:tricarbonyl(η-cyclopentadienyl)(2,3,4,5-tetraphenylstibolyl)molybdenum
CAS No.:71252-91-0
Molecular Formula:C₃₆H₂₅MoO₃Sb
Molecular Weight:723.283
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tricarbonyl(η-cyclopentadienyl)(2,3,4,5-tetraphenylstibolyl)molybdenum

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Technology Process of tricarbonyl(η-cyclopentadienyl)(2,3,4,5-tetraphenylstibolyl)molybdenum

There total 1 articles about tricarbonyl(η-cyclopentadienyl)(2,3,4,5-tetraphenylstibolyl)molybdenum which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: cyclopentadienylmolybdenum tricarbonyl dimer

: 1-chloro-2,3,4,5-tetraphenylstibole

: 71252-91-0
tricarbonyl(η-cyclopentadienyl)(2,3,4,5-tetraphenylstibolyl)molybdenum

Guidance literature:: With sodium amalgam; In tetrahydrofuran; byproducts: Cl(1-); N2-atmosphere; stirring of Mo-complex soln. with Na-amalgam, removal of amalgam, addn. of stibole, stirring for 1 h; filtration, solvent removal (vac.), recrystn. (hexane); elem. anal.;
DOI:10.1039/DT9790000814

Reference yield: 14.0%

: 71252-91-0
tricarbonyl(η-cyclopentadienyl)(2,3,4,5-tetraphenylstibolyl)molybdenum

: 12128-23-3
tricarbonylcyclopentadienylmolybdenum(II) chloride

: 1-chloro-2,3,4,5-tetraphenylstibole

Guidance literature:: With chlorine; In tetrachloromethane; hexane; N2-atmosphere; addn. of Cl2 soln. (in hexane) to soln. of Mo-complex (inCCl4) at -10°C; solvent removal (25°C, 15 mmHg, sublimation (50°C, 0.01 mmHg);
DOI:10.1039/DT9790000814