C₃₀H₄₅N₇O₉

Base Information

Chemical Name:C₃₀H₄₅N₇O₉
CAS No.:1584149-80-3
Molecular Formula:C₃₀H₄₅N₇O₉
Molecular Weight:647.729
Hs Code.:

C<sub>30</sub>H<sub>45</sub>N<sub>7</sub>O<sub>9</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₀H₄₅N₇O₉

Chemical Property:

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Technology Process of C₃₀H₄₅N₇O₉

There total 3 articles about C₃₀H₄₅N₇O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 14.0%

: 92585-03-0
N-(3-((2,4-dinitrophenyl)amino)propyl)-N-(3-aminopropyl)methyl amine

: 1584149-78-9
C₁₇H₂₆N₂O₆

: 1584149-80-3
C₃₀H₄₅N₇O₉

Guidance literature:: C₁₇H₂₆N₂O₆; With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; for 0.166667h; Inert atmosphere; Cooling with ice;

N-(3-((2,4-dinitrophenyl)amino)propyl)-N-(3-aminopropyl)methyl amine; In tetrahydrofuran; for 22h; Inert atmosphere; Darkness;
DOI:10.1002/anie.201309135

Reference yield:

: 35661-60-0
Fmoc-Leu-OH

: 1584149-80-3
C₃₀H₄₅N₇O₉

Guidance literature:: Multi-step reaction with 4 steps

1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / water / 0.17 h / Inert atmosphere; Cooling with ice

1.2: Inert atmosphere

2.1: piperidine / N,N-dimethyl-formamide / 0.67 h / Inert atmosphere

3.1: 4-methyl-morpholine; isobutyl chloroformate / ethyl acetate / 0.17 h / -25 °C / Inert atmosphere

3.2: 5 h / -25 °C / Inert atmosphere

4.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 0.17 h / Inert atmosphere; Cooling with ice

4.2: 22 h / Inert atmosphere; Darkness

With piperidine; 4-methyl-morpholine; di-isopropyl azodicarboxylate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triphenylphosphine; isobutyl chloroformate; In tetrahydrofuran; water; ethyl acetate; N,N-dimethyl-formamide; 4.1: |Mitsunobu Displacement;
DOI:10.1002/anie.201309135

Reference yield:

: 1584149-74-5
C₂₆H₃₀N₂O₄

: 1584149-80-3
C₃₀H₄₅N₇O₉

Guidance literature:: Multi-step reaction with 3 steps

1.1: piperidine / N,N-dimethyl-formamide / 0.67 h / Inert atmosphere

2.1: 4-methyl-morpholine; isobutyl chloroformate / ethyl acetate / 0.17 h / -25 °C / Inert atmosphere

2.2: 5 h / -25 °C / Inert atmosphere

3.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 0.17 h / Inert atmosphere; Cooling with ice

3.2: 22 h / Inert atmosphere; Darkness

With piperidine; 4-methyl-morpholine; di-isopropyl azodicarboxylate; triphenylphosphine; isobutyl chloroformate; In tetrahydrofuran; ethyl acetate; N,N-dimethyl-formamide; 3.1: |Mitsunobu Displacement;
DOI:10.1002/anie.201309135