N-(3-(2-amino-6H-1,3,4-thiadiazin-5-yl)-4-(benzyloxy)phenyl)benzamide monohydrobromide

Base Information

Chemical Name:N-(3-(2-amino-6H-1,3,4-thiadiazin-5-yl)-4-(benzyloxy)phenyl)benzamide monohydrobromide
CAS No.:1429022-65-0
Molecular Formula:BrH*C₂₃H₂₀N₄O₂S
Molecular Weight:497.415
Hs Code.:

Synonyms:

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Chemical Property of N-(3-(2-amino-6H-1,3,4-thiadiazin-5-yl)-4-(benzyloxy)phenyl)benzamide monohydrobromide

Chemical Property:

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Technology Process of N-(3-(2-amino-6H-1,3,4-thiadiazin-5-yl)-4-(benzyloxy)phenyl)benzamide monohydrobromide

There total 9 articles about N-(3-(2-amino-6H-1,3,4-thiadiazin-5-yl)-4-(benzyloxy)phenyl)benzamide monohydrobromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1429022-42-3
N-(4-(benzyloxy)-3-(2-bromoacetyl)phenyl)benzamide

: 1429022-65-0
N-(3-(2-amino-6H-1,3,4-thiadiazin-5-yl)-4-(benzyloxy)phenyl)benzamide monohydrobromide

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol / Reflux

2: hydrogen bromide / ethanol / 0.5 h / Reflux

With hydrogen bromide; In ethanol;
DOI:10.3390/molecules18033577

Reference yield:

: 100-02-7,78813-13-5,89830-32-0
4-nitro-phenol

: 1429022-65-0
N-(3-(2-amino-6H-1,3,4-thiadiazin-5-yl)-4-(benzyloxy)phenyl)benzamide monohydrobromide

Guidance literature:: Multi-step reaction with 8 steps

1: sodium hydroxide / 90 - 95 °C

2: aluminum (III) chloride / nitrobenzene / 6 h / 140 °C

3: potassium carbonate; potassium iodide; N-benzyl-N,N,N-triethylammonium chloride / acetonitrile; water / 2 h / Reflux

4: tin(II) chloride dihdyrate / ethanol / 3 h / 45 °C

5: triethylamine / dichloromethane / 20 °C

6: copper(ll) bromide / ethanol; chloroform / 2 h / Reflux

7: ethanol / Reflux

8: hydrogen bromide / ethanol / 0.5 h / Reflux

With aluminum (III) chloride; tin(II) chloride dihdyrate; N-benzyl-N,N,N-triethylammonium chloride; hydrogen bromide; potassium carbonate; triethylamine; potassium iodide; sodium hydroxide; copper(ll) bromide; In ethanol; dichloromethane; chloroform; water; nitrobenzene; acetonitrile;
DOI:10.3390/molecules18033577

Reference yield:

: 830-03-5
4-nitrophenol acetate

: 1429022-65-0
N-(3-(2-amino-6H-1,3,4-thiadiazin-5-yl)-4-(benzyloxy)phenyl)benzamide monohydrobromide

Guidance literature:: Multi-step reaction with 7 steps

1: aluminum (III) chloride / nitrobenzene / 6 h / 140 °C

2: potassium carbonate; potassium iodide; N-benzyl-N,N,N-triethylammonium chloride / acetonitrile; water / 2 h / Reflux

3: tin(II) chloride dihdyrate / ethanol / 3 h / 45 °C

4: triethylamine / dichloromethane / 20 °C

5: copper(ll) bromide / ethanol; chloroform / 2 h / Reflux

6: ethanol / Reflux

7: hydrogen bromide / ethanol / 0.5 h / Reflux

With aluminum (III) chloride; tin(II) chloride dihdyrate; N-benzyl-N,N,N-triethylammonium chloride; hydrogen bromide; potassium carbonate; triethylamine; potassium iodide; copper(ll) bromide; In ethanol; dichloromethane; chloroform; water; nitrobenzene; acetonitrile;
DOI:10.3390/molecules18033577