C₄₆H₅₃NO₁₀

Base Information

Chemical Name:C₄₆H₅₃NO₁₀
CAS No.:1402588-78-6
Molecular Formula:C₄₆H₅₃NO₁₀
Molecular Weight:779.928
Hs Code.:

C<sub>46</sub>H<sub>53</sub>NO<sub>10</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₆H₅₃NO₁₀

Chemical Property:

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Technology Process of C₄₆H₅₃NO₁₀

There total 14 articles about C₄₆H₅₃NO₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₈H₂₄O₅

: 1402588-78-6
C₄₆H₅₃NO₁₀

: C₄₆H₅₃NO₁₀

Guidance literature:: Multi-step reaction with 3 steps

1: N,N’-(1R,2R)-cyclohexane-1,2-diylbis(1,1,1-trifluoromethanesulfonamide); titanium(IV)isopropoxide / toluene / 8 h / -10 °C / Inert atmosphere

2: Dess-Martin periodane / 2 h / Inert atmosphere

3: phenylborondichloride; N-ethyl-N,N-diisopropylamine / dichloromethane; methanol / 3.5 h / -78 °C / Inert atmosphere

With phenylborondichloride; titanium(IV)isopropoxide; Dess-Martin periodane; N,N’-(1R,2R)-cyclohexane-1,2-diylbis(1,1,1-trifluoromethanesulfonamide); N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane; toluene;
DOI:10.1021/ja3057612

Reference yield:

: 38064-90-3
2,4-dimethoxytoluene

: 1402588-78-6
C₄₆H₅₃NO₁₀

: C₄₆H₅₃NO₁₀

Guidance literature:: Multi-step reaction with 11 steps

1: 6 h / 0 °C / Inert atmosphere

2: Inert atmosphere

3: thionyl chloride / benzene / 2 h / Reflux

4: 0 - 20 °C / Inert atmosphere

5: sec.-butyllithium / cyclohexane / 1 h / -78 °C / Inert atmosphere

6: boron tribromide / dichloromethane / 5.5 h / -78 - 25 °C / Inert atmosphere

7: dichloromethane / 20 h / 20 °C / Inert atmosphere

8: potassium carbonate / N,N-dimethyl-formamide / 20 h / 80 °C / Inert atmosphere

9: 4-methylmorpholine N-oxide; osmium(VIII) oxide / tetrahydrofuran; tert-butyl alcohol; water / 12 h / Inert atmosphere

10: sodium periodate / methanol / 1 h / 20 °C / Inert atmosphere

11: phenylborondichloride; N-ethyl-N,N-diisopropylamine / dichloromethane; methanol / 3.5 h / -78 °C / Inert atmosphere

With sodium periodate; osmium(VIII) oxide; thionyl chloride; phenylborondichloride; sec.-butyllithium; boron tribromide; potassium carbonate; 4-methylmorpholine N-oxide; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; dichloromethane; cyclohexane; water; N,N-dimethyl-formamide; tert-butyl alcohol; benzene;
DOI:10.1021/ja3057612

Reference yield:

: 7149-91-9
2,4-dimethoxy-5-methyl-benzaldehyde

: 1402588-78-6
C₄₆H₅₃NO₁₀

: C₄₆H₅₃NO₁₀

Guidance literature:: Multi-step reaction with 10 steps

1: Inert atmosphere

2: thionyl chloride / benzene / 2 h / Reflux

3: 0 - 20 °C / Inert atmosphere

4: sec.-butyllithium / cyclohexane / 1 h / -78 °C / Inert atmosphere

5: boron tribromide / dichloromethane / 5.5 h / -78 - 25 °C / Inert atmosphere

6: dichloromethane / 20 h / 20 °C / Inert atmosphere

7: potassium carbonate / N,N-dimethyl-formamide / 20 h / 80 °C / Inert atmosphere

8: 4-methylmorpholine N-oxide; osmium(VIII) oxide / tetrahydrofuran; tert-butyl alcohol; water / 12 h / Inert atmosphere

9: sodium periodate / methanol / 1 h / 20 °C / Inert atmosphere

10: phenylborondichloride; N-ethyl-N,N-diisopropylamine / dichloromethane; methanol / 3.5 h / -78 °C / Inert atmosphere

With sodium periodate; osmium(VIII) oxide; thionyl chloride; phenylborondichloride; sec.-butyllithium; boron tribromide; potassium carbonate; 4-methylmorpholine N-oxide; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; dichloromethane; cyclohexane; water; N,N-dimethyl-formamide; tert-butyl alcohol; benzene;
DOI:10.1021/ja3057612