[Th(2,6-bis(2,6-diisopropylanilidomethyl)pyridine)2]

Base Information

Chemical Name:[Th(2,6-bis(2,6-diisopropylanilidomethyl)pyridine)2]
CAS No.:927674-72-4
Molecular Formula:C₆₂H₈₂N₆Th
Molecular Weight:1143.41
Hs Code.:

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Chemical Property of [Th(2,6-bis(2,6-diisopropylanilidomethyl)pyridine)2]

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Technology Process of [Th(2,6-bis(2,6-diisopropylanilidomethyl)pyridine)2]

There total 3 articles about [Th(2,6-bis(2,6-diisopropylanilidomethyl)pyridine)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 184640-73-1
2,6-bis(2,6-bis((2,6-diisopropylphenyl)amino)methyl)pyridine

: 927674-70-2
[(2,6-bis(2,6-diisopropylanilidomethyl)pyridine)Th(CH₂SiMe₃)2]

: 927674-72-4
[Th(2,6-bis(2,6-diisopropylanilidomethyl)pyridine)2]

Guidance literature:: In benzene; Sonication; under Ar atm. Th complex and ligand in benzene were heated at 100°C for 24 h in sealed flask; react. mixt. was cooled and filtered, soln. was concd. in vacuo, hexamethyldisiloxane was added followed by sonication;
DOI:10.1021/om060914f

Reference yield: 26.0%

: 639084-65-4
[ThCl₄(1,2-dimethoxyethane)₂]

: Li₂[2,6-bis(2,6-diisopropylanilidomethyl)pyridine]

: 927674-72-4
[Th(2,6-bis(2,6-diisopropylanilidomethyl)pyridine)2]

Guidance literature:: In benzene; under Ar atm. ThCl4(dme)2 and Li salt ligand in benzene were stirred at 0°C for 1 h; react. mixt. was warmed to room temp. and filtered, solvent was removed in vacuo, hexane was added followed by sonication, ppt. was filtered andwashed with hexane, recrystn. from hot toluene to -30°C; elem. a nal.;
DOI:10.1021/om060914f