C₁₄H₁₆N₄O₄

Base Information

Chemical Name:C₁₄H₁₆N₄O₄
CAS No.:1380481-73-1
Molecular Formula:C₁₄H₁₆N₄O₄
Molecular Weight:304.305
Hs Code.:

C<sub>14</sub>H<sub>16</sub>N<sub>4</sub>O<sub>4</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₄H₁₆N₄O₄

Chemical Property:

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Technology Process of C₁₄H₁₆N₄O₄

There total 6 articles about C₁₄H₁₆N₄O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1380347-94-3
5-amino-3-benzyl-1-methyl-1H-pyrazole-4-carbonitrile

: 1380481-73-1
C₁₄H₁₆N₄O₄

Guidance literature:: Multi-step reaction with 6 steps

1: sodium hydroxide; water / Reflux

2: sodium nitrite; tetrafluoroboric acid / water

3: dimethylsulfide borane complex / tetrahydrofuran / -20 °C / Reflux

4: carbon tetrabromide; triphenylphosphine / dichloromethane

5: O-allyl-N-(9-anthracenylmethyl)cinchonidinium bromide; cesiumhydroxide monohydrate / dichloromethane / -30 °C

6: trifluoroacetic acid / dichloromethane

With tetrafluoroboric acid; cesiumhydroxide monohydrate; carbon tetrabromide; dimethylsulfide borane complex; O-allyl-N-(9-anthracenylmethyl)cinchonidinium bromide; water; triphenylphosphine; trifluoroacetic acid; sodium hydroxide; sodium nitrite; In tetrahydrofuran; dichloromethane; water;
DOI:10.1016/j.bmcl.2013.02.039

Reference yield:

: 1268522-40-2
5-amino-3-benzyl-1-methyl-1H-pyrazole-4-carboxylic acid

: 1380481-73-1
C₁₄H₁₆N₄O₄

Guidance literature:: Multi-step reaction with 5 steps

1: sodium nitrite; tetrafluoroboric acid / water

2: dimethylsulfide borane complex / tetrahydrofuran / -20 °C / Reflux

3: carbon tetrabromide; triphenylphosphine / dichloromethane

4: O-allyl-N-(9-anthracenylmethyl)cinchonidinium bromide; cesiumhydroxide monohydrate / dichloromethane / -30 °C

5: trifluoroacetic acid / dichloromethane

With tetrafluoroboric acid; cesiumhydroxide monohydrate; carbon tetrabromide; dimethylsulfide borane complex; O-allyl-N-(9-anthracenylmethyl)cinchonidinium bromide; triphenylphosphine; trifluoroacetic acid; sodium nitrite; In tetrahydrofuran; dichloromethane; water;
DOI:10.1016/j.bmcl.2013.02.039

Reference yield:

: 42754-59-6
2-(1-Methoxy-2-phenylethylidene)malononitrile

: 1380481-73-1
C₁₄H₁₆N₄O₄

Guidance literature:: Multi-step reaction with 7 steps

1: ethanol / Reflux

2: sodium hydroxide; water / Reflux

3: sodium nitrite; tetrafluoroboric acid / water

4: dimethylsulfide borane complex / tetrahydrofuran / -20 °C / Reflux

5: carbon tetrabromide; triphenylphosphine / dichloromethane

6: O-allyl-N-(9-anthracenylmethyl)cinchonidinium bromide; cesiumhydroxide monohydrate / dichloromethane / -30 °C

7: trifluoroacetic acid / dichloromethane

With tetrafluoroboric acid; cesiumhydroxide monohydrate; carbon tetrabromide; dimethylsulfide borane complex; O-allyl-N-(9-anthracenylmethyl)cinchonidinium bromide; water; triphenylphosphine; trifluoroacetic acid; sodium hydroxide; sodium nitrite; In tetrahydrofuran; ethanol; dichloromethane; water;
DOI:10.1016/j.bmcl.2013.02.039