(4-methoxyphenyl)triethoxygermane

Base Information

Chemical Name:(4-methoxyphenyl)triethoxygermane
CAS No.:249300-81-0
Molecular Formula:C₁₃H₂₂GeO₄
Molecular Weight:314.905
Hs Code.:

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Chemical Property of (4-methoxyphenyl)triethoxygermane

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Technology Process of (4-methoxyphenyl)triethoxygermane

There total 1 articles about (4-methoxyphenyl)triethoxygermane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 104-92-7
1-bromo-4-methoxy-benzene

: 14165-55-0
tetraethoxygermanium

: 249300-81-0
(4-methoxyphenyl)triethoxygermane

Guidance literature:: With Mg; In tetrahydrofuran; byproducts: Mg(OEt)Br; N2-atmosphere; slowly addn. of soln. of 1 equiv. of bromoanisole to mixt. (THF) of Ge(OEt)4 and excess of Mg at reflux, refluxing for 2 h; cooling, addn. of pentane, filtration, evapn., extn. (pentane), evapn.; elem. anal.;
DOI:10.1021/om990349z

Reference yield: 86.4%

: 16853-85-3
lithium aluminium tetrahydride

: 249300-81-0
(4-methoxyphenyl)triethoxygermane

: 21364-14-7
(4-methoxyphenyl)germane

Guidance literature:: In diethyl ether; byproducts: LiOEt, Al(OEt)3; N2-atmosphere; addn. of soln. of Ge-compound to suspension of LiAlH4 at -78°C, stirring for 1 h, warming to room temp.; addn. of pentane, filtration, distillation (68°C, 0.05 mbar); elem. anal.;
DOI:10.1021/om990349z