(1-phenyldibenzophosphole)gold(III)ClBr₂

Base Information

Chemical Name:(1-phenyldibenzophosphole)gold(III)ClBr₂
CAS No.:139630-62-9
Molecular Formula:C₁₈H₁₃AuBr₂ClP
Molecular Weight:652.502
Hs Code.:

(1-phenyldibenzophosphole)gold(III)ClBr<sub>2</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1-phenyldibenzophosphole)gold(III)ClBr₂

Chemical Property:

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Technology Process of (1-phenyldibenzophosphole)gold(III)ClBr₂

There total 4 articles about (1-phenyldibenzophosphole)gold(III)ClBr₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.2%

: 124605-44-3
chloro-1-phenyl-dibenzophosphole gold(I)

: 138897-47-9,139630-62-9,139683-91-3
(1-phenyldibenzophosphole)gold(III)ClBr₂

Guidance literature:: With Br₂; In chloroform; (N2); react. soln. was stirred at ambient temp. for 3 h; filtered; volume reduced; addn. of anhyd. diethyl ether; cooled to 0°C (pptn.); filtered, washed with anhyd. diethyl ether; dried in vac.; elem. anal.;
DOI:10.1016/S0277-5387(00)86058-1

Reference yield:

: 124605-46-5
(DBP)3AuBr

: 139630-62-9,138897-47-9,139683-91-3
trans-((1-phenyldibenzophosphole)gold(III)ClBr₂)

Guidance literature:: Multi-step reaction with 2 steps

1: Br₂ / chloroform

2: chloroform-d1

With Br₂; In chloroform-d1; chloroform;
DOI:10.1016/S0277-5387(00)86058-1

Reference yield:

: 124605-46-5
(DBP)3AuBr

: 14243-66-4
(triphenylphosphine) gold(III) trichloride

: 139630-62-9
cis-((1-phenyldibenzophosphole)gold(III)ClBr₂)

: 138917-07-4
(1-phenyldibenzophosphole)gold(III)Br₃

Guidance literature:: In chloroform-d1; react. of equimolar mixt. under N2 at 30°C; further products; not isolated, 31P-NMR;
DOI:10.1016/S0277-5387(00)86058-1