C₂₄H₂₉N₅O₇S

Base Information

• Chemical Name: C₂₄H₂₉N₅O₇S
• CAS No.: 441797-11-1
• Molecular Formula: C₂₄H₂₉N₅O₇S
• Molecular Weight: 531.59
• Mol file: 441797-11-1.mol

Synonyms:

Chemical Property of C₂₄H₂₉N₅O₇S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₄H₂₉N₅O₇S

There total 5 articles about C₂₄H₂₉N₅O₇S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C22H24ClN5O5S + ethylene glycol (107-21-1) → C24H29N5O7S (441797-11-1)

Guidance literature:

ethylene glycol; With potassium tert-butylate; In 1,2-dimethoxyethane; at 40 ℃; for 0.166667h;

C₂₂H₂₄ClN₅O₅S; In 1,2-dimethoxyethane; at 100 ℃; for 70h;

DOI:10.1021/jm3009103

Reference yield:

methyl (2-methoxyphenoxy) ethanoate (38768-62-6) → C24H29N5O7S (441797-11-1)

Guidance literature:

Multi-step reaction with 5 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 5 h / 40 - 45 °C

1.2: 24 h / 20 - 32 °C

2.1: sodium methylate / methanol / 6 h / 0 - 20 °C

2.2: 72 h / 20 °C

3.1: trichlorophosphate; N-ethyl-N,N-diisopropylamine / 0 - 130 °C

4.1: dimethyl sulfoxide / 48 h / 20 °C

5.1: potassium tert-butylate / 1,2-dimethoxyethane / 0.17 h / 40 °C

5.2: 70 h / 100 °C

With potassium tert-butylate; sodium methylate; sodium hydride; N-ethyl-N,N-diisopropylamine; trichlorophosphate; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; dimethyl sulfoxide; mineral oil;

DOI:10.1021/jm3009103

Reference yield:

(2-methoxyphenoxy)acetic acid (1878-85-9) → C24H29N5O7S (441797-11-1)

Guidance literature:

Multi-step reaction with 6 steps

1.1: thionyl chloride / 3 h / 0 - 20 °C

2.1: sodium hydride / tetrahydrofuran; mineral oil / 5 h / 40 - 45 °C

2.2: 24 h / 20 - 32 °C

3.1: sodium methylate / methanol / 6 h / 0 - 20 °C

3.2: 72 h / 20 °C

4.1: trichlorophosphate; N-ethyl-N,N-diisopropylamine / 0 - 130 °C

5.1: dimethyl sulfoxide / 48 h / 20 °C

6.1: potassium tert-butylate / 1,2-dimethoxyethane / 0.17 h / 40 °C

6.2: 70 h / 100 °C

With thionyl chloride; potassium tert-butylate; sodium methylate; sodium hydride; N-ethyl-N,N-diisopropylamine; trichlorophosphate; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; dimethyl sulfoxide; mineral oil;

DOI:10.1021/jm3009103

upstream raw materials:

methyl (2-methoxyphenoxy) ethanoate

(2-methoxyphenoxy)acetic acid

ethylene glycol

4,6-dichloro-5-(2-methoxy-phenoxy)-2-(morpholin-4-yl)pyrimidine

Downstream raw materials:

C₂₈H₃₀BrN₇O₇S