Technology Process of benzyl 4-O-benzyl-2,3-di-O-ethyl-β-D-glucopyranoside
There total 6 articles about benzyl 4-O-benzyl-2,3-di-O-ethyl-β-D-glucopyranoside which
guide to synthetic route it.
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synthetic route:
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30607-98-8,35905-28-3,40983-94-6,56341-65-2,57783-86-5,58006-32-9,72869-10-4,73366-72-0,79549-73-8,110850-30-1,113973-86-7,117895-05-3
benzyl 4,6-O-benzylidene-β-D-glucopyranoside
- Guidance literature:
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Multi-step reaction with 2 steps
1: 85 percent / silver oxide / dimethylformamide; CHCl3 / 18 h / Ambient temperature
2: 1.) lithium aluminium hydride, aluminium chloride; 2.) ethyl acetate / 1.) ether, dichloromethane, reflux, 2 h.
With
lithium aluminium tetrahydride; aluminium trichloride; ethyl acetate; silver(l) oxide;
In
chloroform; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(00)82220-X
- Guidance literature:
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Multi-step reaction with 4 steps
1: 49 percent / M sodium methoxide, zinc chloride / methanol; CHCl3
2: 14 percent / lithium aluminium hydride / tetrahydrofuran; H2O; ethyl acetate / 7 h / Heating
3: 85 percent / silver oxide / dimethylformamide; CHCl3 / 18 h / Ambient temperature
4: 1.) lithium aluminium hydride, aluminium chloride; 2.) ethyl acetate / 1.) ether, dichloromethane, reflux, 2 h.
With
lithium aluminium tetrahydride; aluminium trichloride; sodium methylate; ethyl acetate; zinc(II) chloride; silver(l) oxide;
In
tetrahydrofuran; methanol; chloroform; water; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(00)82220-X
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 14 percent / lithium aluminium hydride / tetrahydrofuran; H2O; ethyl acetate / 7 h / Heating
2: 85 percent / silver oxide / dimethylformamide; CHCl3 / 18 h / Ambient temperature
3: 1.) lithium aluminium hydride, aluminium chloride; 2.) ethyl acetate / 1.) ether, dichloromethane, reflux, 2 h.
With
lithium aluminium tetrahydride; aluminium trichloride; ethyl acetate; silver(l) oxide;
In
tetrahydrofuran; chloroform; water; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(00)82220-X