Technology Process of C28H36O5
There total 5 articles about C28H36O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: aq. sodium hydrogen phosphate, aq. peroxyacetic acid / CHCl3 / 2 h
2: 87 percent / 72percent aq. perchloric acid / dioxane; acetone / 3 h
3: 2.) H2SO4 / 1.) reflux, 2.) a) 30 deg C, 30 min, b) 20 deg C, 2 h
4: 82 percent / conc. HCl / methanol; CHCl3 / 60 h / 35 °C
5: p-toluenesulfonic acid / benzene / 6 h / Heating
With
hydrogenchloride; peracetic acid; disodium hydrogenphosphate; perchloric acid; sulfuric acid; toluene-4-sulfonic acid;
In
1,4-dioxane; methanol; chloroform; acetone; benzene;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 2.) H2SO4 / 1.) reflux, 2.) a) 30 deg C, 30 min, b) 20 deg C, 2 h
2: 82 percent / conc. HCl / methanol; CHCl3 / 60 h / 35 °C
3: p-toluenesulfonic acid / benzene / 6 h / Heating
With
hydrogenchloride; sulfuric acid; toluene-4-sulfonic acid;
In
methanol; chloroform; benzene;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 87 percent / 72percent aq. perchloric acid / dioxane; acetone / 3 h
2: 2.) H2SO4 / 1.) reflux, 2.) a) 30 deg C, 30 min, b) 20 deg C, 2 h
3: 82 percent / conc. HCl / methanol; CHCl3 / 60 h / 35 °C
4: p-toluenesulfonic acid / benzene / 6 h / Heating
With
hydrogenchloride; perchloric acid; sulfuric acid; toluene-4-sulfonic acid;
In
1,4-dioxane; methanol; chloroform; acetone; benzene;