p-nitrobenzoate of erythro-dihydro-4-ethyl-3-hydroxy-4-methyl-2(3H)-furanone

Base Information

Chemical Name:p-nitrobenzoate of erythro-dihydro-4-ethyl-3-hydroxy-4-methyl-2(3H)-furanone
CAS No.:134734-34-2
Molecular Formula:C₁₄H₁₅NO₆
Molecular Weight:293.276
Hs Code.:

Synonyms:

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Chemical Property of p-nitrobenzoate of erythro-dihydro-4-ethyl-3-hydroxy-4-methyl-2(3H)-furanone

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Technology Process of p-nitrobenzoate of erythro-dihydro-4-ethyl-3-hydroxy-4-methyl-2(3H)-furanone

There total 17 articles about p-nitrobenzoate of erythro-dihydro-4-ethyl-3-hydroxy-4-methyl-2(3H)-furanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 134734-31-9
p-nitrobenzoate of erythro-3-ethyl-4-hydroxy-5-methoxy-3-methyltetrahydrofuran

: 134734-34-2,134734-36-4
p-nitrobenzoate of erythro-dihydro-4-ethyl-3-hydroxy-4-methyl-2(3H)-furanone

Guidance literature:: With boron trifluoride diethyl etherate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; for 3h; Ambient temperature;
DOI:10.1002/jhet.5570280315

Reference yield:

: 134936-48-4
3-Ethyl-2,3-dihydro-furan-3-carboxylic acid methyl ester

: 134734-34-2,134734-36-4
p-nitrobenzoate of erythro-dihydro-4-ethyl-3-hydroxy-4-methyl-2(3H)-furanone

Guidance literature:: Multi-step reaction with 7 steps

1: m-chloroperbenzoic acid / 1 h / 0 °C

2: pyridine / Ambient temperature

3: 95 percent / LiAlH₄ / diethyl ether / 3 h / Heating

4: 61 percent / pyridine / Ambient temperature

5: 31 percent / LiAlH₄ / tetrahydrofuran / 5 h / Heating

6: 97 percent / pyridine / Ambient temperature

7: 90 percent / BF₃*Et₂O, MCPBA / CH₂Cl₂ / 3 h / Ambient temperature

With pyridine; lithium aluminium tetrahydride; boron trifluoride diethyl etherate; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1002/jhet.5570280315

Reference yield:

: methyl 4-hydroxy-5-methoxy-3-ethyltetrahydrofuran-3-carboxylate

: 134734-34-2,134734-36-4
p-nitrobenzoate of erythro-dihydro-4-ethyl-3-hydroxy-4-methyl-2(3H)-furanone

Guidance literature:: Multi-step reaction with 6 steps

1: pyridine / Ambient temperature

2: 95 percent / LiAlH₄ / diethyl ether / 3 h / Heating

3: 61 percent / pyridine / Ambient temperature

4: 31 percent / LiAlH₄ / tetrahydrofuran / 5 h / Heating

5: 97 percent / pyridine / Ambient temperature

6: 90 percent / BF₃*Et₂O, MCPBA / CH₂Cl₂ / 3 h / Ambient temperature

With pyridine; lithium aluminium tetrahydride; boron trifluoride diethyl etherate; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1002/jhet.5570280315