p-nitrobenzoate of erythro-3-ethyl-4-hydroxy-5-methoxy-3-methyltetrahydrofuran

Base Information

Chemical Name:p-nitrobenzoate of erythro-3-ethyl-4-hydroxy-5-methoxy-3-methyltetrahydrofuran
CAS No.:134734-31-9
Molecular Formula:C₁₅H₁₉NO₆
Molecular Weight:309.319
Hs Code.:

Synonyms:p-nitrobenzoate of erythro-3-ethyl-4-hydroxy-5-methoxy-3-methyltetrahydrofuran

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Chemical Property of p-nitrobenzoate of erythro-3-ethyl-4-hydroxy-5-methoxy-3-methyltetrahydrofuran

Chemical Property:

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Technology Process of p-nitrobenzoate of erythro-3-ethyl-4-hydroxy-5-methoxy-3-methyltetrahydrofuran

There total 13 articles about p-nitrobenzoate of erythro-3-ethyl-4-hydroxy-5-methoxy-3-methyltetrahydrofuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 122-04-3
4-nitro-benzoyl chloride

: 134734-29-5,134734-35-3
erythro-3-ethyl-4-hydroxy-5-methoxy-3-methyltetrahydrofuran

: 134734-31-9
p-nitrobenzoate of erythro-3-ethyl-4-hydroxy-5-methoxy-3-methyltetrahydrofuran

Guidance literature:: With pyridine; Ambient temperature;
DOI:10.1002/jhet.5570280315

Reference yield:

: 134936-48-4
3-Ethyl-2,3-dihydro-furan-3-carboxylic acid methyl ester

: 134734-31-9
p-nitrobenzoate of erythro-3-ethyl-4-hydroxy-5-methoxy-3-methyltetrahydrofuran

Guidance literature:: Multi-step reaction with 6 steps

1: m-chloroperbenzoic acid / 1 h / 0 °C

2: pyridine / Ambient temperature

3: 95 percent / LiAlH₄ / diethyl ether / 3 h / Heating

4: 61 percent / pyridine / Ambient temperature

5: 31 percent / LiAlH₄ / tetrahydrofuran / 5 h / Heating

6: 97 percent / pyridine / Ambient temperature

With pyridine; lithium aluminium tetrahydride; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; diethyl ether;
DOI:10.1002/jhet.5570280315

Reference yield:

: methyl 4-hydroxy-5-methoxy-3-ethyltetrahydrofuran-3-carboxylate

: 134734-31-9
p-nitrobenzoate of erythro-3-ethyl-4-hydroxy-5-methoxy-3-methyltetrahydrofuran

Guidance literature:: Multi-step reaction with 5 steps

1: pyridine / Ambient temperature

2: 95 percent / LiAlH₄ / diethyl ether / 3 h / Heating

3: 61 percent / pyridine / Ambient temperature

4: 31 percent / LiAlH₄ / tetrahydrofuran / 5 h / Heating

5: 97 percent / pyridine / Ambient temperature

With pyridine; lithium aluminium tetrahydride; In tetrahydrofuran; diethyl ether;
DOI:10.1002/jhet.5570280315