(1''R,2'R,4S,5'S)-4-<<(diphenylisopropoxy)silyl>oxy>-4-<5'-<1''-<(tert-butyldimethylsilyl)oxy>ethyl>-2',3',4',5'-tetrahydro-5'-methylfuran-2'-yl>pentyl ethanoate

Base Information

Chemical Name:(1''R,2'R,4S,5'S)-4-<<(diphenylisopropoxy)silyl>oxy>-4-<5'-<1''-<(tert-butyldimethylsilyl)oxy>ethyl>-2',3',4',5'-tetrahydro-5'-methylfuran-2'-yl>pentyl ethanoate
CAS No.:128329-39-5
Molecular Formula:C₃₅H₅₆O₆Si₂
Molecular Weight:628.997
Hs Code.:

(1''R,2'R,4S,5'S)-4-<<(diphenylisopropoxy)silyl>oxy>-4-<5'-<1''-<(tert-butyldimethylsilyl)oxy>ethyl>-2',3',4',5'-tetrahydro-5'-methylfuran-2'-yl>pentyl ethanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1''R,2'R,4S,5'S)-4-<<(diphenylisopropoxy)silyl>oxy>-4-<5'-<1''-<(tert-butyldimethylsilyl)oxy>ethyl>-2',3',4',5'-tetrahydro-5'-methylfuran-2'-yl>pentyl ethanoate

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Technology Process of (1''R,2'R,4S,5'S)-4-<<(diphenylisopropoxy)silyl>oxy>-4-<5'-<1''-<(tert-butyldimethylsilyl)oxy>ethyl>-2',3',4',5'-tetrahydro-5'-methylfuran-2'-yl>pentyl ethanoate

There total 2 articles about (1''R,2'R,4S,5'S)-4-<<(diphenylisopropoxy)silyl>oxy>-4-<5'-<1''-<(tert-butyldimethylsilyl)oxy>ethyl>-2',3',4',5'-tetrahydro-5'-methylfuran-2'-yl>pentyl ethanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 114058-14-9
diphenylisopropoxysilyl chloride

: 128329-38-4,128440-34-6
Acetic acid 4-{(2R,5S)-5-[(R)-1-(tert-butyl-dimethyl-silanyloxy)-ethyl]-5-methyl-tetrahydro-furan-2-yl}-4-hydroxy-pentyl ester

: 128329-39-5,128443-27-6
Acetic acid (R)-4-{(2R,5S)-5-[(R)-1-(tert-butyl-dimethyl-silanyloxy)-ethyl]-5-methyl-tetrahydro-furan-2-yl}-4-(isopropoxy-diphenyl-silanyloxy)-pentyl ester

: 128329-39-5,128443-27-6
(1''R,2'R,4S,5'S)-4-<<(diphenylisopropoxy)silyl>oxy>-4-<5'-<1''-<(tert-butyldimethylsilyl)oxy>ethyl>-2',3',4',5'-tetrahydro-5'-methylfuran-2'-yl>pentyl ethanoate

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; for 20h; Yield given. Yields of byproduct given. Title compound not separated from byproducts; Ambient temperature;
DOI:10.1021/ja00169a041

Reference yield:

: 114058-14-9
diphenylisopropoxysilyl chloride

: 128329-38-4,128440-34-6
Acetic acid 4-{(2R,5S)-5-[(R)-1-(tert-butyl-dimethyl-silanyloxy)-ethyl]-5-methyl-tetrahydro-furan-2-yl}-4-hydroxy-pentyl ester

: 128329-39-5,128443-27-6
Acetic acid (R)-4-{(2R,5S)-5-[(R)-1-(tert-butyl-dimethyl-silanyloxy)-ethyl]-5-methyl-tetrahydro-furan-2-yl}-4-(isopropoxy-diphenyl-silanyloxy)-pentyl ester

: 128329-39-5,128443-27-6
(1''R,2'R,4S,5'S)-4-<<(diphenylisopropoxy)silyl>oxy>-4-<5'-<1''-<(tert-butyldimethylsilyl)oxy>ethyl>-2',3',4',5'-tetrahydro-5'-methylfuran-2'-yl>pentyl ethanoate

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; for 20h; Yield given. Yields of byproduct given. Title compound not separated from byproducts; Ambient temperature;
DOI:10.1021/ja00169a041