(R)-4-(Benzyloxycarbonylmethyl-amino)-2-{[(R)-3-benzyloxycarbonyl-3-(tetrahydro-pyran-2-yloxy)-propyl]-tert-butoxycarbonyl-amino}-butyric acid benzyl ester

Base Information

• Chemical Name: (R)-4-(Benzyloxycarbonylmethyl-amino)-2-{[(R)-3-benzyloxycarbonyl-3-(tetrahydro-pyran-2-yloxy)-propyl]-tert-butoxycarbonyl-amino}-butyric acid benzyl ester
• CAS No.: 120926-61-6
• Molecular Formula: C₄₁H₅₂N₂O₁₀
• Molecular Weight: 732.871

Synonyms:

Chemical Property of (R)-4-(Benzyloxycarbonylmethyl-amino)-2-{[(R)-3-benzyloxycarbonyl-3-(tetrahydro-pyran-2-yloxy)-propyl]-tert-butoxycarbonyl-amino}-butyric acid benzyl ester

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of (R)-4-(Benzyloxycarbonylmethyl-amino)-2-{[(R)-3-benzyloxycarbonyl-3-(tetrahydro-pyran-2-yloxy)-propyl]-tert-butoxycarbonyl-amino}-butyric acid benzyl ester

There total 6 articles about (R)-4-(Benzyloxycarbonylmethyl-amino)-2-{[(R)-3-benzyloxycarbonyl-3-(tetrahydro-pyran-2-yloxy)-propyl]-tert-butoxycarbonyl-amino}-butyric acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzyl bromide (100-39-0) → (R)-4-(Benzyloxycarbonylmethyl-amino)-2-{[(R)-3-benzyloxycarbonyl-3-(tetrahydro-pyran-2-yloxy)-propyl]-tert-butoxycarbonyl-amino}-butyric acid benzyl ester (120926-61-6)

Guidance literature:

Multi-step reaction with 2 steps

2: NaBH₃CN

With sodium cyanoborohydride;

DOI:10.1021/ja00191a055

Reference yield:

3,4-dihydro-2H-pyran (110-87-2) → (R)-4-(Benzyloxycarbonylmethyl-amino)-2-{[(R)-3-benzyloxycarbonyl-3-(tetrahydro-pyran-2-yloxy)-propyl]-tert-butoxycarbonyl-amino}-butyric acid benzyl ester (120926-61-6)

Guidance literature:

Multi-step reaction with 4 steps

2: NaBH₃CN

4: NaBH₃CN

With sodium cyanoborohydride;

DOI:10.1021/ja00191a055

Reference yield:

di-tert-butyl dicarbonate (24424-99-5) → (R)-4-(Benzyloxycarbonylmethyl-amino)-2-{[(R)-3-benzyloxycarbonyl-3-(tetrahydro-pyran-2-yloxy)-propyl]-tert-butoxycarbonyl-amino}-butyric acid benzyl ester (120926-61-6)

Guidance literature:

Multi-step reaction with 2 steps

2: NaBH₃CN

With sodium cyanoborohydride;

DOI:10.1021/ja00191a055

upstream raw materials:

glycine benzyl ester trifluoroacetic salt

(R)-2-{[(R)-3-Benzyloxycarbonyl-3-(tetrahydro-pyran-2-yloxy)-propyl]-tert-butoxycarbonyl-amino}-4-oxo-butyric acid benzyl ester

3,4-dihydro-2H-pyran

di-tert-butyl dicarbonate

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