triacontane-1,30-diol

Base Information

• Chemical Name: triacontane-1,30-diol
• CAS No.: 36645-68-8
• Molecular Formula: C₃₀H₆₂O₂
• Molecular Weight: 454.821
• Mol file: 36645-68-8.mol

Synonyms:

Chemical Property of triacontane-1,30-diol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of triacontane-1,30-diol

There total 13 articles about triacontane-1,30-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

triaconta-1,29-diene (947504-74-7) → triacontane-1,30-diol (36645-68-8)

Guidance literature:

triaconta-1,29-diene; With diisoamyl borane; In tetrahydrofuran; at 20 ℃;

With sodium hydroxide; dihydrogen peroxide; In tetrahydrofuran; ethanol; at 50 ℃; for 3h; Further stages.;

DOI:10.1002/chem.200601866

Reference yield:

ω-bromo-1-[(tetrahydro-2H-pyran-2-yl)oxy]pentadecane (103687-89-4) + p-Xylylene dichloride (623-25-6) → triacontane-1,30-diol (36645-68-8) + 2,2'-[1,4-phenylenebis(hexadecane-16,1-diyloxy)]bis(tetrahydro-2H-pyran)

Guidance literature:

ω-bromo-1-[(tetrahydro-2H-pyran-2-yl)oxy]pentadecane; With magnesium; In tetrahydrofuran; at 50 ℃; for 2h; Inert atmosphere;

p-Xylylene dichloride; With dilithium tetrachlorocuprate; In tetrahydrofuran; at 0 ℃; for 3h; Inert atmosphere;

DOI:10.1007/s00706-012-0833-2

Reference yield:

1,4-bis(bromomethyl)benzene (623-24-5) + ω-bromo-1-[(tetrahydro-2H-pyran-2-yl)oxy]pentadecane (103687-89-4) → triacontane-1,30-diol (36645-68-8) + 2,2'-[1,4-phenylenebis(hexadecane-16,1-diyloxy)]bis(tetrahydro-2H-pyran)

Guidance literature:

ω-bromo-1-[(tetrahydro-2H-pyran-2-yl)oxy]pentadecane; With magnesium; In tetrahydrofuran; at 50 ℃; for 2h; Inert atmosphere;

1,4-bis(bromomethyl)benzene; With dilithium tetrachlorocuprate; In tetrahydrofuran; at 0 ℃; for 3h; Inert atmosphere;

DOI:10.1007/s00706-012-0833-2

upstream raw materials:

triaconta-1,29-diene

pentadecanolide

1,8-dibromooctane

methyl 15-hydroxypentadecanoate