methyl epiphorellate 2

Base Information

Chemical Name:methyl epiphorellate 2
CAS No.:101910-78-5
Molecular Formula:C₂₇H₃₄O₉
Molecular Weight:502.562
Hs Code.:

Synonyms:

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Chemical Property of methyl epiphorellate 2

Chemical Property:

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Technology Process of methyl epiphorellate 2

There total 22 articles about methyl epiphorellate 2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24131-31-5
3,5-dibenzyloxybenzyl alcohol

: 101910-78-5
methyl epiphorellate 2

Guidance literature:: Multi-step reaction with 16 steps

1: 95 percent / thionyl chloride, pyridine / CH₂Cl₂ / 3 h / Ambient temperature

2: 88 percent / dimethylformamide / 7 h / Ambient temperature

3: 91 percent / 30percent aq. sodium hydroxide / methanol / 72 h / Heating

4: 95 percent / potassium carbonate / acetone / 3 h / Heating

5: 95 percent / lithium aluminium hydride / diethyl ether / 2 h / Heating

6: 85 percent / pyridine / CHCl₃ / 3 h / 0 °C

7: 94 percent / 1,2-dimethoxyethane / dimethylsulfoxide / 18 h / Ambient temperature

8: 81 percent / ether / benzene / 1 h / Ambient temperature; aq. hydrochloric acid, ethyl acetate, 16 h

9: 98 percent / trifluoroacetic anhydride, / nitromethane / 1.5 h / 0 °C

10: 81 percent / H₂, conc. hydrochloric acid (4 drops) / 10percent palladized charcoal / ethyl acetate

11: 73 percent / potassium cyanoferrate(III), potassium carbonate / H₂O; dioxane / 0.17 h

12: 70 percent / various solvent(s) / 0.17 h / Heating

13: 94 percent / potassium carbonate / dimethylformamide / Ambient temperature

14: 66 percent / sodium methoxide / methanol / 3 h / Ambient temperature

15: 82 percent / potassium carbonate / dimethylformamide / 5 h / Ambient temperature

16: 1.) boron trichloride, 2.) H₂ / 10percent palladized chacoal / 1.) dichloromethane, -10 deg C, 0.5 h, 2.) ethyl acetate, conc. hydrochloric acid (1 drop)

With pyridine; hydrogenchloride; sodium hydroxide; lithium aluminium tetrahydride; 1,2-dimethoxyethane; thionyl chloride; diethyl ether; hydrogen; sodium methylate; boron trichloride; potassium carbonate; trifluoroacetic anhydride; potassium hexacyanoferrate(III); palladium on activated charcoal; In 1,4-dioxane; methanol; diethyl ether; nitromethane; dichloromethane; chloroform; water; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide; acetone; benzene;

Reference yield:

: 58016-28-7
methyl 2,6-dihydroxy-6-pentylbenzoate

: 101910-78-5
methyl epiphorellate 2

Guidance literature:: Multi-step reaction with 12 steps

1: 77 percent / potassium carbonate / acetone / 24 h / Heating

2: 89 percent / potassium carbonate / acetone / Heating

3: 80 percent / phosphoryl chloride / 24 h / 70 °C

4: 97 percent / sodium chlorite, sulphamic acid / H₂O; dioxane / 0.67 h

5: 98 percent / trifluoroacetic anhydride, / nitromethane / 1.5 h / 0 °C

6: 81 percent / H₂, conc. hydrochloric acid (4 drops) / 10percent palladized charcoal / ethyl acetate

7: 73 percent / potassium cyanoferrate(III), potassium carbonate / H₂O; dioxane / 0.17 h

8: 70 percent / various solvent(s) / 0.17 h / Heating

9: 94 percent / potassium carbonate / dimethylformamide / Ambient temperature

10: 66 percent / sodium methoxide / methanol / 3 h / Ambient temperature

11: 82 percent / potassium carbonate / dimethylformamide / 5 h / Ambient temperature

12: 1.) boron trichloride, 2.) H₂ / 10percent palladized chacoal / 1.) dichloromethane, -10 deg C, 0.5 h, 2.) ethyl acetate, conc. hydrochloric acid (1 drop)

With hydrogenchloride; sodium chlorite; aminosulfonic acid; hydrogen; sodium methylate; boron trichloride; potassium carbonate; trifluoroacetic anhydride; potassium hexacyanoferrate(III); trichlorophosphate; palladium on activated charcoal; In 1,4-dioxane; methanol; nitromethane; water; ethyl acetate; N,N-dimethyl-formamide; acetone;

Reference yield:

: 2732-96-9
3,5-dibenzyloxyphenylacetic acid

: 101910-78-5
methyl epiphorellate 2

Guidance literature:: Multi-step reaction with 13 steps

1: 95 percent / potassium carbonate / acetone / 3 h / Heating

2: 95 percent / lithium aluminium hydride / diethyl ether / 2 h / Heating

3: 85 percent / pyridine / CHCl₃ / 3 h / 0 °C

4: 94 percent / 1,2-dimethoxyethane / dimethylsulfoxide / 18 h / Ambient temperature

5: 81 percent / ether / benzene / 1 h / Ambient temperature; aq. hydrochloric acid, ethyl acetate, 16 h

6: 98 percent / trifluoroacetic anhydride, / nitromethane / 1.5 h / 0 °C

7: 81 percent / H₂, conc. hydrochloric acid (4 drops) / 10percent palladized charcoal / ethyl acetate

8: 73 percent / potassium cyanoferrate(III), potassium carbonate / H₂O; dioxane / 0.17 h

9: 70 percent / various solvent(s) / 0.17 h / Heating

10: 94 percent / potassium carbonate / dimethylformamide / Ambient temperature

11: 66 percent / sodium methoxide / methanol / 3 h / Ambient temperature

12: 82 percent / potassium carbonate / dimethylformamide / 5 h / Ambient temperature

13: 1.) boron trichloride, 2.) H₂ / 10percent palladized chacoal / 1.) dichloromethane, -10 deg C, 0.5 h, 2.) ethyl acetate, conc. hydrochloric acid (1 drop)

With pyridine; hydrogenchloride; lithium aluminium tetrahydride; 1,2-dimethoxyethane; diethyl ether; hydrogen; sodium methylate; boron trichloride; potassium carbonate; trifluoroacetic anhydride; potassium hexacyanoferrate(III); palladium on activated charcoal; In 1,4-dioxane; methanol; diethyl ether; nitromethane; chloroform; water; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide; acetone; benzene;