Technology Process of C45H66O5Si
There total 4 articles about C45H66O5Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
silver hexafluoroantimonate; 2-(2-(4,5-dihydrooxazol-2-yl)propan-2-yl)-4,5-dihydrooxazole; copper(ll) bromide;
In
dichloromethane;
at 20 ℃;
optical yield given as %de;
diastereoselective reaction;
Inert atmosphere;
Molecular sieve;
DOI:10.1002/chem.201103495
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / Inert atmosphere
1.2: Inert atmosphere
2.1: silver hexafluoroantimonate; 2-(2-(4,5-dihydrooxazol-2-yl)propan-2-yl)-4,5-dihydrooxazole; copper(ll) bromide / dichloromethane / 20 °C / Inert atmosphere; Molecular sieve
With
silver hexafluoroantimonate; 2-(2-(4,5-dihydrooxazol-2-yl)propan-2-yl)-4,5-dihydrooxazole; sodium hydride; copper(ll) bromide;
In
dichloromethane; N,N-dimethyl-formamide; mineral oil;
DOI:10.1002/chem.201103495
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: piperdinium acetate / benzene / 18 h / Reflux; Inert atmosphere
2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / Inert atmosphere
2.2: Inert atmosphere
3.1: silver hexafluoroantimonate; 2-(2-(4,5-dihydrooxazol-2-yl)propan-2-yl)-4,5-dihydrooxazole; copper(ll) bromide / dichloromethane / 20 °C / Inert atmosphere; Molecular sieve
With
silver hexafluoroantimonate; 2-(2-(4,5-dihydrooxazol-2-yl)propan-2-yl)-4,5-dihydrooxazole; piperdinium acetate; sodium hydride; copper(ll) bromide;
In
dichloromethane; N,N-dimethyl-formamide; mineral oil; benzene;
DOI:10.1002/chem.201103495
