3,3-Dipropylcyclobutanone toluene-p-sulfonylhydrazone

Base Information

Chemical Name:3,3-Dipropylcyclobutanone toluene-p-sulfonylhydrazone
CAS No.:215957-72-5
Molecular Formula:C₁₇H₂₆N₂O₂S
Molecular Weight:322.472
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,3-Dipropylcyclobutanone toluene-p-sulfonylhydrazone

Chemical Property:

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Technology Process of 3,3-Dipropylcyclobutanone toluene-p-sulfonylhydrazone

There total 3 articles about 3,3-Dipropylcyclobutanone toluene-p-sulfonylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 123-19-3
4-heptanone

: 215957-72-5
3,3-Dipropylcyclobutanone toluene-p-sulfonylhydrazone

Guidance literature:: Multi-step reaction with 4 steps

1: 60 percent / Sodium hydride / dimethylsulfoxide / 2 h / 50 °C

2: 73 percent / zinc dust / diethyl ether / 1 h / sonication

3: 92 percent / zinc dust / acetic acid / 0.83 h / 70 °C

4: 74 percent / tetrahydrofuran

With sodium hydride; zinc; In tetrahydrofuran; diethyl ether; acetic acid; dimethyl sulfoxide; 1: Wittig reaction / 2: Cycloaddition / 3: Dehalogenation / 4: Condensation;

Reference yield:

: 15918-08-8
2-propyl-1-pentene

: 215957-72-5
3,3-Dipropylcyclobutanone toluene-p-sulfonylhydrazone

Guidance literature:: Multi-step reaction with 3 steps

1: 73 percent / zinc dust / diethyl ether / 1 h / sonication

2: 92 percent / zinc dust / acetic acid / 0.83 h / 70 °C

3: 74 percent / tetrahydrofuran

With zinc; In tetrahydrofuran; diethyl ether; acetic acid; 1: Cycloaddition / 2: Dehalogenation / 3: Condensation;

Reference yield:

: 215957-59-8
2,2-dichloro-3,3-dipropylcyclobutanone

: 215957-72-5
3,3-Dipropylcyclobutanone toluene-p-sulfonylhydrazone

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / zinc dust / acetic acid / 0.83 h / 70 °C

2: 74 percent / tetrahydrofuran

With zinc; In tetrahydrofuran; acetic acid; 1: Dehalogenation / 2: Condensation;