8-chloro-6-(2-chlorophenyl)-1-{[4-(2-phenoxyethyl)-1-piperazinyl]methyl}-4H-[1,2,4]triazolo[4,3-a][1,4]benzodiazepine

Base Information

Chemical Name:8-chloro-6-(2-chlorophenyl)-1-{[4-(2-phenoxyethyl)-1-piperazinyl]methyl}-4H-[1,2,4]triazolo[4,3-a][1,4]benzodiazepine
CAS No.:89719-83-5
Molecular Formula:C₂₉H₂₈Cl₂N₆O
Molecular Weight:547.487
Hs Code.:
Mol file:89719-83-5.mol

Synonyms:

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Chemical Property of 8-chloro-6-(2-chlorophenyl)-1-{[4-(2-phenoxyethyl)-1-piperazinyl]methyl}-4H-[1,2,4]triazolo[4,3-a][1,4]benzodiazepine

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Technology Process of 8-chloro-6-(2-chlorophenyl)-1-{[4-(2-phenoxyethyl)-1-piperazinyl]methyl}-4H-[1,2,4]triazolo[4,3-a][1,4]benzodiazepine

There total 4 articles about 8-chloro-6-(2-chlorophenyl)-1-{[4-(2-phenoxyethyl)-1-piperazinyl]methyl}-4H-[1,2,4]triazolo[4,3-a][1,4]benzodiazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 589-10-6
phenoxyethyl bromide

: 89719-83-5
8-Chloro-6-(2-chloro-phenyl)-1-[4-(2-phenoxy-ethyl)-piperazin-1-ylmethyl]-4H-2,3,5,10b-tetraaza-benzo[e]azulene

Guidance literature:: Multi-step reaction with 3 steps

1: 53 percent / K₂CO₃ / acetone / 6 h / Heating

2: 56 percent / N₂H₄H₂O / ethanol / 8 h / Heating

3: butan-1-ol / 10 h / Heating

With potassium carbonate; hydrazine hydrate; In ethanol; acetone; butan-1-ol;
DOI:10.1135/cccc19833433

Reference yield:

: 40004-08-8
1-(Ethoxycarbonylmethyl)piperazine

: 89719-83-5
8-Chloro-6-(2-chloro-phenyl)-1-[4-(2-phenoxy-ethyl)-piperazin-1-ylmethyl]-4H-2,3,5,10b-tetraaza-benzo[e]azulene

Guidance literature:: Multi-step reaction with 3 steps

1: 53 percent / K₂CO₃ / acetone / 6 h / Heating

2: 56 percent / N₂H₄H₂O / ethanol / 8 h / Heating

3: butan-1-ol / 10 h / Heating

With potassium carbonate; hydrazine hydrate; In ethanol; acetone; butan-1-ol;
DOI:10.1135/cccc19833433

Reference yield:

: 48190-66-5
[4-(2-phenoxy-ethyl)-piperazin-1-yl]-acetic acid ethyl ester

: 89719-83-5
8-Chloro-6-(2-chloro-phenyl)-1-[4-(2-phenoxy-ethyl)-piperazin-1-ylmethyl]-4H-2,3,5,10b-tetraaza-benzo[e]azulene

Guidance literature:: Multi-step reaction with 2 steps

1: 56 percent / N₂H₄H₂O / ethanol / 8 h / Heating

2: butan-1-ol / 10 h / Heating

With hydrazine hydrate; In ethanol; butan-1-ol;
DOI:10.1135/cccc19833433