2,3-dihydro-6,7-bis(hydroxymethyl)-5-phenylsulfonyl-1H-pyrrolizine bis-

Base Information

Chemical Name:2,3-dihydro-6,7-bis(hydroxymethyl)-5-phenylsulfonyl-1H-pyrrolizine bis-
CAS No.:129503-37-3
Molecular Formula:C₂₃H₃₁N₃O₆S
Molecular Weight:477.582
Hs Code.:

2,3-dihydro-6,7-bis(hydroxymethyl)-5-phenylsulfonyl-1H-pyrrolizine bis-<N-(2-propyl)carbamate>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,3-dihydro-6,7-bis(hydroxymethyl)-5-phenylsulfonyl-1H-pyrrolizine bis-

Chemical Property:

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Technology Process of 2,3-dihydro-6,7-bis(hydroxymethyl)-5-phenylsulfonyl-1H-pyrrolizine bis-

There total 4 articles about 2,3-dihydro-6,7-bis(hydroxymethyl)-5-phenylsulfonyl-1H-pyrrolizine bis- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 62563-06-8
dimethyl 2,3-dihydro-1H-pyrrolizine-6,7-dicarboxylate

: 129503-37-3
2,3-dihydro-6,7-bis(hydroxymethyl)-5-phenylsulfonyl-1H-pyrrolizine bis-

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / CH₂Cl₂ / 0.25 h / Ambient temperature

2: 52 percent / 1.) 31percent H₂O₂, conc. H₂SO₄, glac. HOAc / 1.) rt, 24 h, 2.) 50 deg C, 24 h

With sulfuric acid; dihydrogen peroxide; acetic acid; In dichloromethane;
DOI:10.1002/jhet.5570270440

Reference yield:

: 931-59-9
benzenesulfenyl chloride

: 129503-37-3
2,3-dihydro-6,7-bis(hydroxymethyl)-5-phenylsulfonyl-1H-pyrrolizine bis-

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / CH₂Cl₂ / 0.25 h / Ambient temperature

2: 52 percent / 1.) 31percent H₂O₂, conc. H₂SO₄, glac. HOAc / 1.) rt, 24 h, 2.) 50 deg C, 24 h

With sulfuric acid; dihydrogen peroxide; acetic acid; In dichloromethane;
DOI:10.1002/jhet.5570270440

Reference yield:

: 129503-31-7
dimethyl 2,3-dihydro-5-phenylthio-1H-pyrrolizine-6,7-dicarboxylate

: 129503-37-3
2,3-dihydro-6,7-bis(hydroxymethyl)-5-phenylsulfonyl-1H-pyrrolizine bis-

Guidance literature:: Multi-step reaction with 2 steps

1: 52 percent / 1.) 31percent H₂O₂, conc. H₂SO₄, glac. HOAc / 1.) rt, 24 h, 2.) 50 deg C, 24 h

With sulfuric acid; dihydrogen peroxide; acetic acid;
DOI:10.1002/jhet.5570270440