N,N',N''-tris(2-methylphenyl)borazine

Base Information

Chemical Name:N,N',N''-tris(2-methylphenyl)borazine
CAS No.:38798-80-0
Molecular Formula:C₂₁H₂₄B₃N₃
Molecular Weight:350.875
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N',N''-tris(2-methylphenyl)borazine

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Technology Process of N,N',N''-tris(2-methylphenyl)borazine

There total 3 articles about N,N',N''-tris(2-methylphenyl)borazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: triethylamine borane

: 95-53-4
o-toluidine

: 38798-80-0
N,N',N''-tris(2-methylphenyl)borazine

Guidance literature:: In neat (no solvent); byproducts: Et3N; The aniline-compd. is added slowly to Et3NBH3 at 100°C with stirring under Ar (pyrolysis), the temp. is raised to 200°C with evolution of Et3N.; cooling, recrystn. (C6H6/hexane);

Reference yield: 45.0%

: 5775-58-6
1,3,5-tri-o-tolyl-2,4,6-trichloro borazine

: 38798-80-0
N,N',N''-tris(2-methylphenyl)borazine

Guidance literature:: With lithium aluminium tetrahydride; ammonium chloride; In diethyl ether; reducing agent addn. in small portions to suspension of B-compd., boiling (5 h), saturated soln. of NH4Cl addn. (0°C); solvent removing, washing with water, drying over MgSO4, evapn. to dryness, residue re-crystn. (hexane); elem. anal.;