B,B',B''-trimethyl-N,N',N''-tris(2-methylphenyl)borazine

Base Information

Chemical Name:B,B',B''-trimethyl-N,N',N''-tris(2-methylphenyl)borazine
CAS No.:749-85-9
Molecular Formula:C₂₄H₃₀B₃N₃
Molecular Weight:392.955
Hs Code.:

Synonyms:B,B',B''-trimethyl-N,N',N''-tris(2-methylphenyl)borazine

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Chemical Property of B,B',B''-trimethyl-N,N',N''-tris(2-methylphenyl)borazine

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Technology Process of B,B',B''-trimethyl-N,N',N''-tris(2-methylphenyl)borazine

There total 7 articles about B,B',B''-trimethyl-N,N',N''-tris(2-methylphenyl)borazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 917-64-6
methyl magnesium iodide

: 2,4-dibromo-8-methyl-3-o-tolyl-2,4-dibora-1,3-diaza-naphthalene

: 749-85-9
B,B',B''-trimethyl-N,N',N''-tris(2-methylphenyl)borazine

: 42168-28-5
2,4-dimethyl-3-o-tolyl-8-methyl-2,4-dibora-1,3-diazaronaphthalene

Guidance literature:: With ammonium chloride; In diethyl ether; (under N2) to an ether soln. of MeMgI is added the dibromodiboradiazanaphthalenederiv., mixt. is refluxed for 1 h, soln. is hydrolyzed with NH4Cl; white crystals are isolated, VPC yields two components, main compd. is recrystd. from water-MeOH, elem. anal.;

Reference yield: 60.0%

: 126295-21-4
B,B',B''-trifluoro-N,N',N''-tris(2-methylphenyl)borazine

: 749-85-9
B,B',B''-trimethyl-N,N',N''-tris(2-methylphenyl)borazine

Guidance literature:: With CH₃MgI; In diethyl ether; To a diethyl ether soln. of MeMgI crude (o-MeC6H4NBF)3 is added by small portions, the mixture is refluxed for 1 h under Ar.; the mixture is cooled with an ice-bath and quenched with NH4Cl in H2O, addn. of methanol, a 33/67 cis/trans-mixture is obtained, sepn. of isomers not possible;