8-(dimesitylboryl)-1-methylquinolinium triflate

Base Information

Chemical Name:8-(dimesitylboryl)-1-methylquinolinium triflate
CAS No.:1260019-80-4
Molecular Formula:CF₃O₃S*C₂₈H₃₁BN
Molecular Weight:541.442
Hs Code.:

Synonyms:

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Chemical Property of 8-(dimesitylboryl)-1-methylquinolinium triflate

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Technology Process of 8-(dimesitylboryl)-1-methylquinolinium triflate

There total 4 articles about 8-(dimesitylboryl)-1-methylquinolinium triflate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1260019-76-8
8-(dimesitylboryl)quinoline

: 333-27-7
methyl trifluoromethanesulfonate

: 1260019-80-4
8-(dimesitylboryl)-1-methylquinolinium triflate

Guidance literature:: In dichloromethane; (N2); addn. of methyl triflate to CH2Cl2 soln. of quinoline deriv., stirring; evapn., elem. anal.;
DOI:10.1039/c0dt00798f

Reference yield:

: 16567-18-3
8-bromoquinoline

: 1260019-80-4
8-(dimesitylboryl)-1-methylquinolinium triflate

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / -78 °C / Inert atmosphere

1.2: -78 - 20 °C / Inert atmosphere

2.1: dichloromethane / Inert atmosphere

With n-butyllithium; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1039/c0dt00798f

Reference yield:

: 1006-47-9
iodo-8 quinoleine

: 1260019-80-4
8-(dimesitylboryl)-1-methylquinolinium triflate

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / -78 °C / Inert atmosphere

1.2: -78 - 20 °C / Inert atmosphere

2.1: dichloromethane / Inert atmosphere

With n-butyllithium; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1039/c0dt00798f