C₂₆H₂₆ClN₃O₂

Base Information

Chemical Name:C₂₆H₂₆ClN₃O₂
CAS No.:1450652-71-7
Molecular Formula:C₂₆H₂₆ClN₃O₂
Molecular Weight:447.964
Hs Code.:

C<sub>26</sub>H<sub>26</sub>ClN<sub>3</sub>O<sub>2</sub>

Synonyms:

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Chemical Property of C₂₆H₂₆ClN₃O₂

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Technology Process of C₂₆H₂₆ClN₃O₂

There total 3 articles about C₂₆H₂₆ClN₃O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 53855-47-3
ethyl 2-methyl-1H-indole-3-carboxylate

: 1450652-71-7
C₂₆H₂₆ClN₃O₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 50 - 60 °C / Inert atmosphere

1.2: 0 - 20 °C

2.1: potassium hydroxide; water / methanol / Reflux

3.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; triethylamine / dichloromethane / 0.5 h / 20 °C / Inert atmosphere

3.2: 20 °C

With water; sodium hydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; potassium hydroxide; In methanol; dichloromethane; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 615-43-0
2-iodophenylamine

: 1450652-71-7
C₂₆H₂₆ClN₃O₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: copper(I) oxide; caesium carbonate / water; dimethyl sulfoxide / 16 h / 100 °C / Inert atmosphere

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 50 - 60 °C / Inert atmosphere

2.2: 0 - 20 °C

3.1: potassium hydroxide; water / methanol / Reflux

4.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; triethylamine / dichloromethane / 0.5 h / 20 °C / Inert atmosphere

4.2: 20 °C

With copper(I) oxide; water; sodium hydride; benzotriazol-1-ol; caesium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; potassium hydroxide; In methanol; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 1450659-45-6
ethyl 1-(1-(4-chlorophenyl)ethyl)-2-methyl-1H-indole-3-carboxylate

: 1450652-71-7
C₂₆H₂₆ClN₃O₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hydroxide; water / methanol / Reflux

2.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; triethylamine / dichloromethane / 0.5 h / 20 °C / Inert atmosphere

2.2: 20 °C

With water; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; potassium hydroxide; In methanol; dichloromethane;