methyl 2-deoxy-2-phthalimido-β-D-glucopyranosyl-(1->4)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

Base Information

Chemical Name:methyl 2-deoxy-2-phthalimido-β-D-glucopyranosyl-(1->4)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside
CAS No.:1371585-26-0
Molecular Formula:C₄₃H₄₂N₂O₁₃
Molecular Weight:794.812
Hs Code.:

Synonyms:

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Chemical Property of methyl 2-deoxy-2-phthalimido-β-D-glucopyranosyl-(1->4)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

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Technology Process of methyl 2-deoxy-2-phthalimido-β-D-glucopyranosyl-(1->4)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

There total 11 articles about methyl 2-deoxy-2-phthalimido-β-D-glucopyranosyl-(1->4)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 85-44-9
phthalic anhydride

: 1371585-26-0
methyl 2-deoxy-2-phthalimido-β-D-glucopyranosyl-(1->4)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 10 steps

1.1: sodium hydroxide / water / 20 °C

2.1: pyridine / 0 - 20 °C

3.1: boron trifluoride diethyl etherate / chloroform / 0.17 h / 0 - 20 °C / Inert atmosphere

3.2: 2 h / 20 °C / Inert atmosphere

4.1: methanol; sodium methylate / 1.5 h / 20 °C / pH 9

5.1: toluene-4-sulfonic acid / N,N-dimethyl-formamide / 20 - 50 °C

6.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / Inert atmosphere

6.2: 20 °C / Inert atmosphere

7.1: hydrogenchloride; sodium cyanoborohydride / tetrahydrofuran; diethyl ether / 5 h / 0 - 20 °C / Molecular sieve

8.1: N-iodo-succinimide; silver trifluoromethanesulfonate / dichloromethane / 0.17 h / 20 °C / Inert atmosphere

9.1: N-iodo-succinimide; silver trifluoromethanesulfonate / dichloromethane / 0.25 h / 20 °C / Molecular sieve; Inert atmosphere

10.1: methanol; sodium methylate / 0.5 h / 20 °C / pH 9 - 10

With pyridine; hydrogenchloride; methanol; N-iodo-succinimide; boron trifluoride diethyl etherate; sodium methylate; silver trifluoromethanesulfonate; sodium hydride; sodium cyanoborohydride; toluene-4-sulfonic acid; sodium hydroxide; In tetrahydrofuran; diethyl ether; dichloromethane; chloroform; water; N,N-dimethyl-formamide; mineral oil;
DOI:10.1039/c2ob07066a

Reference yield:

: 1078691-95-8
(+)-D-glucosamine hydrochloride

: 1371585-26-0
methyl 2-deoxy-2-phthalimido-β-D-glucopyranosyl-(1->4)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 10 steps

1.1: sodium hydroxide / water / 20 °C

2.1: pyridine / 0 - 20 °C

3.1: boron trifluoride diethyl etherate / chloroform / 0.17 h / 0 - 20 °C / Inert atmosphere

3.2: 2 h / 20 °C / Inert atmosphere

4.1: methanol; sodium methylate / 1.5 h / 20 °C / pH 9

5.1: toluene-4-sulfonic acid / N,N-dimethyl-formamide / 20 - 50 °C

6.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / Inert atmosphere

6.2: 20 °C / Inert atmosphere

7.1: hydrogenchloride; sodium cyanoborohydride / tetrahydrofuran; diethyl ether / 5 h / 0 - 20 °C / Molecular sieve

8.1: N-iodo-succinimide; silver trifluoromethanesulfonate / dichloromethane / 0.17 h / 20 °C / Inert atmosphere

9.1: N-iodo-succinimide; silver trifluoromethanesulfonate / dichloromethane / 0.25 h / 20 °C / Molecular sieve; Inert atmosphere

10.1: methanol; sodium methylate / 0.5 h / 20 °C / pH 9 - 10

With pyridine; hydrogenchloride; methanol; N-iodo-succinimide; boron trifluoride diethyl etherate; sodium methylate; silver trifluoromethanesulfonate; sodium hydride; sodium cyanoborohydride; toluene-4-sulfonic acid; sodium hydroxide; In tetrahydrofuran; diethyl ether; dichloromethane; chloroform; water; N,N-dimethyl-formamide; mineral oil;
DOI:10.1039/c2ob07066a

Reference yield:

: 31505-42-7
2-(2-carboxybenzamido)-2-deoxy-D-glucopyranose

: 1371585-26-0
methyl 2-deoxy-2-phthalimido-β-D-glucopyranosyl-(1->4)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1.1: pyridine / 0 - 20 °C

2.1: boron trifluoride diethyl etherate / chloroform / 0.17 h / 0 - 20 °C / Inert atmosphere

2.2: 2 h / 20 °C / Inert atmosphere

3.1: N-iodo-succinimide; silver trifluoromethanesulfonate / dichloromethane / 0.25 h / 20 °C / Molecular sieve; Inert atmosphere

4.1: methanol; sodium methylate / 0.5 h / 20 °C / pH 9 - 10

With pyridine; methanol; N-iodo-succinimide; boron trifluoride diethyl etherate; sodium methylate; silver trifluoromethanesulfonate; In dichloromethane; chloroform;
DOI:10.1039/c2ob07066a