Benzyloxycarbonylamino-thioacetic acid S-{2-[2-((2S,3S)-3-{2-[2-(2-benzyloxycarbonylamino-acetylsulfanyl)-ethoxy]-ethoxymethyl}-1,4,7,10,13,16-hexaoxa-cyclooctadec-2-ylmethoxy)-ethoxy]-ethyl} ester

Base Information

Chemical Name:Benzyloxycarbonylamino-thioacetic acid S-{2-[2-((2S,3S)-3-{2-[2-(2-benzyloxycarbonylamino-acetylsulfanyl)-ethoxy]-ethoxymethyl}-1,4,7,10,13,16-hexaoxa-cyclooctadec-2-ylmethoxy)-ethoxy]-ethyl} ester
CAS No.:96454-15-8
Molecular Formula:C₄₂H₆₂N₂O₁₆S₂
Molecular Weight:915.09
Hs Code.:

Benzyloxycarbonylamino-thioacetic acid S-{2-[2-((2S,3S)-3-{2-[2-(2-benzyloxycarbonylamino-acetylsulfanyl)-ethoxy]-ethoxymethyl}-1,4,7,10,13,16-hexaoxa-cyclooctadec-2-ylmethoxy)-ethoxy]-ethyl} ester

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Chemical Property of Benzyloxycarbonylamino-thioacetic acid S-{2-[2-((2S,3S)-3-{2-[2-(2-benzyloxycarbonylamino-acetylsulfanyl)-ethoxy]-ethoxymethyl}-1,4,7,10,13,16-hexaoxa-cyclooctadec-2-ylmethoxy)-ethoxy]-ethyl} ester

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Technology Process of Benzyloxycarbonylamino-thioacetic acid S-{2-[2-((2S,3S)-3-{2-[2-(2-benzyloxycarbonylamino-acetylsulfanyl)-ethoxy]-ethoxymethyl}-1,4,7,10,13,16-hexaoxa-cyclooctadec-2-ylmethoxy)-ethoxy]-ethyl} ester

There total 4 articles about Benzyloxycarbonylamino-thioacetic acid S-{2-[2-((2S,3S)-3-{2-[2-(2-benzyloxycarbonylamino-acetylsulfanyl)-ethoxy]-ethoxymethyl}-1,4,7,10,13,16-hexaoxa-cyclooctadec-2-ylmethoxy)-ethoxy]-ethyl} ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 68394-45-6
(2S,3S)-2,3-Bis(hydroxymethyl)-1,4,7,10,13,16-hexaoxacyclooctadecan

: 96454-15-8
Benzyloxycarbonylamino-thioacetic acid S-{2-[2-((2S,3S)-3-{2-[2-(2-benzyloxycarbonylamino-acetylsulfanyl)-ethoxy]-ethoxymethyl}-1,4,7,10,13,16-hexaoxa-cyclooctadec-2-ylmethoxy)-ethoxy]-ethyl} ester

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) NaH(50 percent in oil) / 1.) DMF, 1 h, room t., then 40 deg C, 1 h, 2.) DMF, room t., 17 h

2: ethanol / 1 h / Heating

3: 5 N NaOH / ethanol / 1 h / 40 °C

4: 1.) Et₃N, diethyl pyrocarbonate 2.) pyridine / 1.) DMF, 0 deg C, 1 h, then room t., 1 h, 2.) room t., 20 min

With pyridine; sodium hydroxide; sodium hydride; triethylamine; diethyl dicarbonate; In ethanol;
DOI:10.1248/cpb.37.912

Reference yield:

: C₃₆H₅₂O₁₂S₂

: 96454-15-8
Benzyloxycarbonylamino-thioacetic acid S-{2-[2-((2S,3S)-3-{2-[2-(2-benzyloxycarbonylamino-acetylsulfanyl)-ethoxy]-ethoxymethyl}-1,4,7,10,13,16-hexaoxa-cyclooctadec-2-ylmethoxy)-ethoxy]-ethyl} ester

Guidance literature:: Multi-step reaction with 2 steps

1: 5 N NaOH / ethanol / 1 h / 40 °C

2: 1.) Et₃N, diethyl pyrocarbonate 2.) pyridine / 1.) DMF, 0 deg C, 1 h, then room t., 1 h, 2.) room t., 20 min

With pyridine; sodium hydroxide; triethylamine; diethyl dicarbonate; In ethanol;
DOI:10.1248/cpb.37.912

Reference yield:

: 125372-55-6
C₃₆H₅₆O₁₆S₂

: 96454-15-8
Benzyloxycarbonylamino-thioacetic acid S-{2-[2-((2S,3S)-3-{2-[2-(2-benzyloxycarbonylamino-acetylsulfanyl)-ethoxy]-ethoxymethyl}-1,4,7,10,13,16-hexaoxa-cyclooctadec-2-ylmethoxy)-ethoxy]-ethyl} ester

Guidance literature:: Multi-step reaction with 3 steps

1: ethanol / 1 h / Heating

2: 5 N NaOH / ethanol / 1 h / 40 °C

3: 1.) Et₃N, diethyl pyrocarbonate 2.) pyridine / 1.) DMF, 0 deg C, 1 h, then room t., 1 h, 2.) room t., 20 min

With pyridine; sodium hydroxide; triethylamine; diethyl dicarbonate; In ethanol;
DOI:10.1248/cpb.37.912